Dear Jan,

 

It is hard to compare refinement results from different refinemnt procedures 
because not all the information you need is stored in the output PDB file. I 
agree with Dirk that you just have to 'pick your own standard'. Provided all 
you models are the output of a converged refinement, you can (e.g.) just do a 
0-cycle run of restrained refinement in Refmac with fixed TLS tensors (if 
applicable).

 

Cheers,

Robbie Joosten
 


Date: Thu, 25 Feb 2010 14:38:02 +0000
From: [email protected]
Subject: [ccp4bb] about comparing Rwork and Rfree factors of different 
refinement trials
To: [email protected]





Dear all,

I do have a question about comparing Rfree and Rwork factors of different 
refinement trials whereas I always started with the same pdb file and structure 
factors (phasing by MR).
Means I had a protein structure which was (not just by me) refined several 
times in different ways also with different programs and also accordingly got 
different R factors for each finally refined structure. 
Could anyone suggest if there is something like a "standard run" which makes 
all these R factors (or "derivatives" since this run should change the R 
factors) better comparable? 
(E.g. it did not work for me to do a 1 cycle rigid body refinement in refmac 
hoping that the R factors are measured well and the structure does not change 
much. In fact, the R factors increased dramatically, lets say Rfree from 30% to 
40%.) 

Many thanks for your suggestions!
Jan

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