I'd worry a bit. If the data are strong and the R factor is that bad you may 
have got your space group wrong (pseudo, not crystallographic 4 fold?)

Pete Artymiuk


On 22 Apr 2010, at 18:22, Frank von Delft wrote:

> Yeah, stop worrying!  Your I/sdI is all that matters.
> phx
> 
> 
> On 22/04/2010 18:06, Daniel Bonsor wrote:
>> Hello again.
>> 
>> At first I was not worry but maybe now I am. I have completed a structure 
>> and submitted to the PDB. They queried my Rsym value in the highest 
>> resolution bin, 2.5-2.37A (may I dare say it 100%). I was not worried at the 
>> time as I had:
>> 
>> 99.4% completeness
>> Mean(I/sdI) of 2.5
>> and a redundancy of 11 (which would explain the high Rsym)
>> Space group I422
>> 
>> My Rpim in this shell is 30%.
>> 
>> Should I reduce the resolution and start from scratch again or is everything 
>> fine and dandy and I should stop worrying?
>>   

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