Dear experts,
Thank you very much for your valuable the suggestions. Dear Tim, the
electron density map is good and fitted well. Krishnaswamy sir, there are
some unmodelled blobs with positive density, I have added respective ions
and refined the model using phenix.refine (Rf- 20.56 and Rfree- 25.76).
Now the question, what is the actual resolution of the data? When I scaled
to 1.7Å resolution the data statistics is as follows:
Rmerge- 25.5 (239)a
I/sigmaI- 10 (3.2)
Completness-100
(100)
Multiplicity 11.8 (12.1)
a - indicate the values in the outer shell (1.7-1.79 Å)
The Rmerge at 3.1 Å resolution is 11.5 % while at 1.7 Å it is 239%. Do I
have enough data to justify 1.7 Å resolution? Are those Rfactor values are
justified with this resolution?Thanking you
DCB
On Sun, Oct 13, 2013 at 12:03 PM, Kay Diederichs <
[email protected]> wrote:
> Are you certain that the data are not twinned?
>
> HTH
>
> Kay
>
>
--
Mr.Dilip C. Badgujar,
Senior Research Fellow,
ACTREC,
Tata Memorial Center,
Sector-22, Kharghar,
Navi Mumbai.
Pin-410210
