Hi Debasish,

I would first use some of those crystals to make seeds and grow some new 
crystals so that I would not lose the crystal. Dehydration, even done 
systematically (eg, 
http://www.mitegen.com/mic_catalog.php?c=jenCrystaloptdehydrate), may or may 
not improve the diffraction. Like most other things in biological 
crystallography, it varies from case to case. I do not think other people’s 
experience really means anything for your crystals.

Zhijie


From: Debasish Chattopadhyay 
Sent: Thursday, February 20, 2014 10:59 AM
To: [email protected] 
Subject: [ccp4bb] Recovering crystals from dry drops

Would you please share your experience and comments on recovering protein 
crystals from dry (or almost dry hanging drops) for data collection.

 

I found some beautiful crystals in hanging drops that were set up three years 
ago; from the color of the crystals ( the protein binds a colored substrate) 
and the their shape I know these are crystals of my protein.  I had collected 
data using some of these crystals when they were fresh; resolution was poor and 
the overall I/sigma was low.  I am curious if the dehydration would improve the 
diffraction now.

 

Thanks

 

Debasish

 

 

 

Ph: (205)934-0124; Fax: (205)934-0480

 

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