A round of refinement with simulated annealing followed by minimization
should address your concern.
Pavel

On Wed, Oct 11, 2017 at 4:48 PM, Karsten Dreifus <[email protected]>
wrote:

> Dear all,
> I have a 120 aa protein. Matthews coefficient indicates 3 mol in asu.
> Molrep (template with 70 % seq identity)  finds three NCS molecules
> (the template model has only 1 chain as it is in different space
> group). Now, REFMAC refines it to 25/30 % R/RFREE. I was just worried
> about model bias, so I just deleted chain C and re-ran the refinement.
> I observe that in the place of chain C, the DELFWT map in Coot shows
> negative density (red colour). Shouldnt the deleted regions show
> POSITIVE density (green colour)? The 2fo-fc map in the deleted region
> shows usual blue colour. I shook the 2chain model with Phenix simple
> dynamics and then ran refinement with same results.
>
> How do I verify the model is correct?
> Karsten
>

Reply via email to