In the Phenix reflection file editor, where you pick the R-free set, there are 
two boxes where you can enter the fraction of reflections to go into the test 
set (see below), but they don't seem to talk to each other. Change the one in 
the "More options" sub-menu and the other stays the same with apparently no 
effect on the calculations.
https://www.ucl.ac.uk/~rmhajc0/phenixrfree.jpg

Also, even if you tick the "Adjust test set size to specified fraction" option, 
it won't allow you to have more than 2000 reflections in your test set (2020 
tops) i.e. there seems to be no way of overriding the "max_free = 2000" command 
with the gui. Probably this is very sensible and I assume it is intended? 

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