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 <A HREF="http://www.delphion.com/details?&pn=US03899144__&s_all=1">Powder
contrail generation (US3899144)</A>
http://www.delphion.com/details?&pn=US03899144__&s_all=1

 US3899144:Powder contrail generation

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Inventor(s): Werle; Donald K. , Hillside, IL
Kasparas; Romas , Riverside, IL
Katz; Sidney , Chicago, IL

Applicant(s): The United States of America as represented by the Secretary of
the Navy, Washington, DC
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Issued/Filed Dates: Aug. 12, 1975 / July 22, 1974


Application Number: US1974000490610


IPC Class: B64D 1/16;


Class: Current: 244/136; 040/213; 116/214; 241/005;
Original: 244/136; 040/213; 116/114.F; 241/005;


Field of Search: 244/136 040/213 241/5,29 222/3;4 239/171 116/28 R,114 R,114
F,114 N,124 R,124 B,124 C


Legal Status: Gazette date Code   Description (remarks)   List all possible
codes for US
Aug. 12, 1975 A  Patent
July 22, 1974 AE  Application data

Abstract:
:
 Light scattering pigment powder particles, surface treated to minimize
inparticle cohesive forces, are dispensed from a jet mill deagglomerator as
separate single particles to produce a powder contrail having maximum
visibility or radiation scattering ability for a given weight material.


Attorney, Agent, or Firm: Sciascia; Richard S.; St. Amand; Joseph M.;


Primary/Assistant Examiners: Blix; Trygve M.; Kelmachter; Barry L.

U.S. References:   Show the 1 patent that references this one Patent   Issued
  Inventor(s)  Applicant(s)   Title
US1619183* 3 /1927  Bradner et al.
US2045865* 6 /1936  Morey
US2591988* 4 /1952  Willcox
US3531310 9 /1970  Goodspeed et al.   PRODUCTION OF IMPROVED METAL OXIDE
PIGMENT
USR0015771* 2 /1924  Savage
  * some details unavailable

CLAIMS:
[Hide claims]: What is claim is:
    1. Contrail generation apparatus for producing a powder contrail having
maximum radiation scattering ability for a given weight material, comprising:
a. an aerodynamic housing;
b. a jet tube means passing through said housing, said tube means having an
inlet at a forward end of said housing and an exhaust at a rearward end
thereof;
c. a powder storage means in said housing;
d. a deagglomeration means also in said housing;
e. means connecting said powder storage means with said deagglomeration means
for feeding radiation scattering powder from said powder storage means to
said deagglomeration means;
f. the output of said deagglomeration means dispensing directly into said jet
tube means for exhausting deagglomerated powder particles into the atmosphere
to form a contrail; and
h. means for controlling the flow of said powder from said storage means to
said deagglomeration means.
    2. Apparatus as in claim 1 wherein said jet tube means is a ram air jet
tube.
    3. Apparatus as in claim 1 wherein an upstream deflector baffle is
provided at the output of said deagglomeration means into said jet tube means
to produce a venturi effect for minimizing back pressure on said powder
feeding means.
    4. Apparatus as in claim 1 wherein said deagglomerator means comprises:
a. means for subjecting powder particles from said powder storage means to a
hammering action to aerate and precondition the powder; and
b. a jet mill means to further deagglomerate the powder into separate
particles.
    5. Apparatus as in claim 4 wherein pressurized gas means is provided for
operating said deagglomeration means.
    6. Apparatus as in claim 1 wherein said radiation scattering powder
particles are titanium dioxide pigment having a median particle size of about
0.3 microns.
    7. Apparatus as in claim 1 wherein said radiation scattering powder
particles have a coating of extremely fine hydrophobic colloidal silica
thereon to minimize interparticle cohesive forces.
    8. Apparatus as in claim 1 wherein the formulation of said powder
consists of 85% by weight of TiO2 pigment of approximately 0.3 micron media
particle size, 10% by weight of colloidal silica of 0.007 micron primary
particle size, and 5% by weight of silica gel having an average particle size
of 4.5 microns.
    9. The method of producing a light radiation scattering contrail,
comprising:
a. surface treating light scattering powder particles to minimize
interparticle cohesive forces;
b. deagglomerating said powder particles in two stages prior to dispensing
into a jet tube by subjecting said powder particles to a hammering action in
the first stage to aerate and precondition the powder, and by passing said
powder through a jet mill in the second stage to further deagglomerate the
powder;
c. dispensing the deagglomerated powder from the jet mill directly into a jet
tube for exhausting said powder into the atmosphere, thus forming a contrail.
    10. A method as in claim 9 wherein said light scattering powder particles
is titanium dioxide pigment.
    11. A method as in claim 9 wherein said powder particles are treated with
a coating of extremely fine hydrophobic colloidal silica to minimize
interparticle cohesive forces.
    12. A method as in claim 11 wherein said treated powder particles are
further protected with a silica gel powder.


Background/Summary:
BACKGROUND

    The present invention relates to method and apparatus for contrail
generation and the like.
    An earlier known method in use for contrail generation involves oil smoke
trails produced by injecting liquid oil directly into the hot jet exhaust of
an aircraft target vehicle. The oil vaporizes and recondenses being the
aircraft producing a brilliant white trail. Oil smoke trail production
requires a minimum of equipment; and, the material is low in cost and readily
available. However, oil smoke requires a heat source to vaporize the liquid
oil and not all aircraft target vehicles, notably towed targets, have such a
heat source. Also, at altitudes above about 25,000 feet oil smoke visibility
degrades rapidly.

SUMMARY

    The present invention is for a powder generator requiring no heat source
to emit a "contrail" with sufficient visibility to aid in visual acquisition
of an aircraft target vehicle and the like. The term "contrail" was adopted
for convenience in identifying the visible powder trail of this invention.
Aircraft target vehicles are used to simulate aerial threats for missile
tests and often fly at altitudes between 5,000 and 20,000 feet at speeds of
300 and 400 knots or more. The present invention is also suitable for use in
other aircraft vehicles to generate contrails or reflective screens for any
desired purpose.
    The powder contail generator is normally carried on an aircraft in a pod
containing a ram air tube and powder feed hopper. Powder particles, surface
treated to minimize interparticle cohesive forces are fed from the hopper to
a deagglomerator and then to the ram air tube for dispensing as separate
single particles to produce a contrail having maximum visibility for a given
weight material.
    Other object, advantages and novel features of the invention will become
apparent from the following detailed description of the invention when
considered in conjunction with the accompanying drawing.


Drawing Descriptions:
DESCRIPTION OF DRAWING

    FIG. 1 is a schematic sectional side-view of a powder contrail generator
of the present invention.


Description of Preferred Embodiments:
DESCRIPTION OF PREFERRED EMBODIMENT

    The powder contail generator in pod 10, shown in FIG. 1, is provided with
a powder feed hopper 12 positioned in the center section of the pod and which
feeds a powder 13 to a deagglomerator 14 by means of screw conveyors 16
across the bottom of the hopper. The deagglomerator 14 produces two stages of
action. In the first stage of deagglomeration, a shaft 18 having projecting
radial rods 19 in compartment 20 is rotated by an air motor 21, or other
suitable drive means. The shaft 18 is rotated at about 10,000 rpm, for
example. As powder 13 descends through the first stage compartment 20 of the
deagglomeration chamber, the hammering action of rotating rods 19 serves to
aerate and precondition the powder before the second stage of deagglomeration
takes place in the jet mill section 22. In the jet mill 22, a plurality of
radial jets 24 (e.g., six 0.050 inch diamter radial jets) direct nitrogen gas
(at e.g., 120 psig) inward to provide energy for further deagglomeration of
the powder. The N2, or other suitable gas, is provided from storage tanks 25
and 26, for example, in the pod.
    The jet mill 22 operates in a similar manner to commercial fluid energy
mills except that there is no provision for recirculation of oversize
particles. Tests with the deagglomerator show that at a feed rate of
approximately 11/2 lb/min, treated titanium dioxide powder pigment is
effectively dispersed as single particles with very few agglomerates evident.
    The nitrogen gas stored in cylinder tanks 25 and 26 is charged to 1800
psig, for example. Two stages of pressure reduction, for example, by pressure
reduction valves 28 and 29, bring the final delivery pressure at the radial
jets 24 and to the air motor 21 to approximately 120 psig. A solenoid valve
30 on the 120 psig line is connected in parallel with the electric motor 32
which operates the powder feeder screws 16 for simultaneous starting and
running of the powder feed, the air motor and the jet mill deagglomerator.
    Air enters ram air tube 34 at its entrance 35 and the exhaust from the
jet mill deagglomerator passes directly into the ram air tube. At the
deagglomerator exhaust 36 into ram air tube 34, an upstream deflector baffle
38 produces a venturi effect which minimizes back pressure on the powder feed
system. The powder is then jetted from the exhaust end 40 of the ram air tube
to produce a contrail. A pressure equalization tube, not shown, can be used
to connect the top of the closed hopper 12 to the deagglomeration chamber 14.
A butterfly valve could be provided at the powder hopper outlet 39 to
completely isolate and seal off the powder supply when not in use. Powder 13
could then be stored in hopper 12 for several weeks, without danger of
picking up excessive moisture, and still be adequately dispensed.
    Preparation of the light scatter powder 13 is of a critical importance to
production of a powder "contrail" having maximum visibility for a given
weight of material. It is essential that the pigment powder particles be
dispensed as separate single particles rather than as agglomerates of two or
more particles. The powder treatment produces the most easily dispersed
powder through the use of surface treatments which minimize interparticle
cohesive forces.
    Titanium dioxide pigment was selected as the primary light scattering
material because of its highly efficient light scattering ability and
commercially available pigment grades. Titanium dioxide pigment (e.g., DuPont
R--931) with a median particle size of about 0.3µ has a high bulk density and
is not readily aerosolizable as a submicron cloud without the consumption of
a large amount of deagglomeration energy. In order to reduce the energy
requirement for deagglomeration, the TiO2 powder is specially treated with a
hydrophobic colloidal silica which coats and separates the individual TiO2
pigment particles. The extremely fine particulate nature (0.007µ primary
particle size) of Cobot S--101 Silanox grade, for example, of colloidal
silica minimizes the amount needed to coat and separate the TiO2 particles,
and the hydrophobic surface minimizes the affinity of the powder for
absorbtion of moisture from the atmosphere. Adsorbed moisture in powders
causes liquid bridges at interparticle contacts and it then becomes necessary
to overcome the adsorbed-liquid surface tension forces as well as the weaker
Van der Waals' forces before the particles can be separated.
    The Silanox treated titanium dioxide pigment is further protected from
the deleterious effects of adsorbed moisture by incorporation of silica gel.
The silica gel preferentially adsorbs water vapor that the powder may be
exposed to after drying and before use. The silica gel used is a powder
product, such as Syloid 65 from the W. R Grace and Co., Davison Chemical
Division, and has an average particle size about 4.5µ and a large capacity
for moisture at low humidities.
    A typical powder composition used is shown in Table 1. This formulation
was blended intimately with a Patterson-Kelley Co. twin shell dry LB-model
LB--2161 with intensifier. Batches of 1500 g were blended for 15 min. each
and packaged in 5-lb cans. The bulk density of the blended powder is 0.22
g/cc. Since deagglomeration is facilitated by having the powder bone dry, the
powder should be predried before sealing the cans. In view of long periods
(e.g., about 4 months) between powder preparation and use it is found
preferable to spread the powder in a thin layer in an open container and
place in a 400°F over two days before planned usage. The powder is removed
and placed in the hopper about 2 hours before use.

Table 1______________________________________CONTRAIL POWDER
FORMULATIONIngredient % by Weight______________________________________TiO2
(e.g., DuPont R-931) 85 median particle size 0.3µColloidal Silica (e.g.,
Cabot S-101 Silanox) 10 primary particle size 0.007µSilica gel (e.g., Syloid
65) 5 average particle size 4.5µ______________________________________

    Other type powder compositions can also be used with the apparatus
described herein. For example, various powder particles which reflect
electromagnetic radiation can be dispensed as a chaff or the like from the
contrail generator.
    Obviously many modifications and variations of the present invention are
possible in the light of the above teachings. It is therefore to be
understood that within the scope of the appended claims the invention may be
practiced otherwise than as specifically described.


Foreign References: Publication Country Date IPC Class
GB01022621  United Kingdom 3 /1966






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