http://onlinelibrary.wiley.com/doi/10.1002/adfm.201202442/abstract

Highly Stable Nanoporous Sulfur-Bridged Covalent Organic Polymers for
Carbon Dioxide Removal - Patel - 2012 - Advanced Functional Materials -
Wiley Online Library

Keywords:

porous polymers;carbon dioxide;thermal stability;adsorption

Abstract

Carbon dioxide capture and separation requires robust solids that can stand
harsh environments where a hot mixture of gases is often found. Herein, the
first and comprehensive syntheses of porous sulfur-bridged covalent organic
polymers (COPs) and their application for carbon dioxide capture in warm
conditions and a wide range of pressures (0-200 bar) are reported. These
COPs can store up to 3294 mg g-1 of carbon dioxide at 318 K and 200 bar
while being highly stable against heating up to 400 °C. The carbon dioxide
capacity of the COPs is also not hindered upon boiling in water for at
least one week. Physisorptive binding is prevalent with isosteric heat of
adsorptions around 24 kJ mol-1. M06-2X and RIMP2 calculations yield the
same relative trend of binding energies, where, interestingly, the dimer of
triazine and benzene play a cooperative role for a stronger binding of
CO2 (19.2 kJ mol-1) as compared to a separate binding with triazine (13.3
kJ mol-1) or benzene (11.8 kJ mol-1).

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