http://www.sciencedirect.com/science/article/pii/S1750583614002898

Journal of Greenhouse Gas Control
December 2014, Vol.31:67–76, doi:10.1016/j.ijggc.2014.09.027

Carbon dioxide removal by using Mg(OH)2 in a bubble column: Effects of
various operating parameters

Tongyan Li
Tim C. Keener
Lei Cheng

Highlights

•The effects of various operating parameters on CO2 removal efficiency were
studied.
•The absorption equilibrium results obtained by MINEQL+ modeling and
experimental data were compared.
•CO2 absorption rates under different conditions were compared.
•The dissolution of Mg(OH)2 and precipitation of MgCO3 in the absorption
process were discussed.

Abstract

The present work includes the absorption of CO2 with Mg(OH)2 slurry in a
bubble column reactor under semi-batch mode. To examine the effects of
operating conditions on CO2absorption performance, several important
parameters including concentration of Mg(OH)2, inlet gas flow rate, and
operating temperature on CO2 absorption behavior were studied. CO2 removal
efficiency and absorption capacity (C:Mg ratio) were used to evaluate the
absorption performance. Carbon dioxide removal efficiency increases with
the increase of liquid height in the column, while the other parameters
affect the efficiency in a more complex way. It is found that absorption
capacity decreases with the increase of Mg(OH)2 concentration due to the
interaction between Mg(OH)2 dissolution and MgCO3precipitation. To observe
the carbon transformation in solid phase, CHNS elemental analyzer was used
to obtain the carbon mass percentage in solid samples. The carbon and
magnesium speciation under equilibrium was modeled with MINEQL+. And the
absorption capacity given by it conforms to the experimental data.

Keywords

CO2 absorption
Magnesium hydroxide dissolution
Bubble column
Magnesium carbonate precipitation
Various operating parameters

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