I think that Shnayer Leiman's Canonization of Hebrew scripture is still one of the standard works on the topic. He also has some very entertaining lectures on the subject at http://www.judaic.org/lectures/lectures.htm although the audio wasn't working when I checked today. You can order the lectures from the Sephardic Institute or http://members.aol.com/TorahShiurim/leiman.htm
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