It's possible that your data really has a kink in it. Zoom in on that last bit in E space before any background subtraction and see if there's something odd-looking. If there's really an artifactual kink, then there's not much you can do.
        mam

On 10/29/2020 7:47 AM, Carlo Segre wrote:
I agree, this is a sign of a poor background subtraction.  I find that this can be mitigated by cutting back on your spl;ine range for background subtraction.  Change it by 0.5 at a time or less and keep plotting in k-space.  You might have to lose a bit of range but that just means that the data is not good enough to extend that far.

Carlo

On Thu, Oct 29, 2020 at 9:23 AM Edmund Welter <edmund.wel...@desy.de <mailto:edmund.wel...@desy.de>> wrote:

    Dear Danting,

    did you look on the background that is subtracted? I guess it is
    your background that is doing something weird here. To look at the
    background tick "Background" in the plot. In the region you mention
    it should be a smooth line without visible oscillations.

    Cheers,

    Edmund


    On 29.10.20 11:02, Chen, Danting wrote:

    Hi Mr/Ms,

    __ __

    I am a new learner of XAS and meet a problem like before and hope
    you can give me some hints.

    __ __

    __ __

    I have a data set after merged and alignment. But at 11-13 A-1,
    the amplitude of k is much higher than normal but there seems no
    weird points at XAS spectrum. I wonder how I could deal with this
    part? If I shorter kmax and it must lose some important information.

    __ __

    Best Wishes,

    Danting

    Sent from Mail <https://go.microsoft.com/fwlink/?LinkId=550986>
    for Windows 10

    __ __


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--
Carlo U. Segre -- Duchossois Leadership Professor of Physics
Director, Center for Synchrotron Radiation Research and Instrumentation
Illinois Institute of Technology
Voice: 312.567.3498            Fax: 312.567.3494
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