Alex,
I wish I had an answer, but I too have that model that has been sitting on a ac 
powered speaker stand next to the bed for the last 7 years. I probably last 
synched it 6 years ago. I have been wondering what would happened if I synched 
it.
Is the battery fully charged?
After searching for similar problems, I found this:

https://discussions.apple.com/thread/2360928?start=0&tstart=0

and the solution back then, in 2010, was to reinstall iTunes (do not uninstall 
first, just reinstall iTunes on top of the current iTunes).

I hope that helps.
Bill

On Aug 5, 2011, at 9:55 PM, Alex Whitman wrote:

> I have an iPod from 2003 or maybe 2004, the 3rd generation, with a touch 
> wheel, 4 buttons and a firewire dock. Today I tried to sync it with iTunes 
> (10.4). No dice - iTunes becomes unresponsive and gives me a spinning beach 
> ball until I force quit. The battery will charge but there is no syncing 
> happening. Tried it without the dock, just the cable, with the same result. 
> This is the first time I've tried to sync it in at least a year, so several 
> iTunes updates have happened since then. Is it simply obsolete? Or is there 
> something else I should try?
> 
> Many thanks,
> Alex
> 
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