Hi rkvs,

Warm welcome to the world of nixies.

The darkening of the tube is part of the manufacturing process and is not 
an indicator these have been used. Shorter leads are also not an indicator, 
sometimes they are trimmed for shipping. In brief, its purpose is to clean 
impurities from the cathode electrode and gas. The front of the tube is 
also affected, but it has been partially shielded by the mesh-type anode. 
The very early and excellent-named 'tuneon' bargraph tube had no such mesh 
and 
look<http://www.radiomuseum.org/forumdata/users/14211/tuneon_brian_001_sml.png> 
at 
it before and after prolonged use.

Alex I think you are referring to traditional 'flashed' getters that leave 
an unmistakable reflective surface on the glass.
I believe the 'non-evaporable' type is used in the IN-9 and IN-13, in the 
form of a sintered metal alloy 'pill' at the very top of the tube. 
Here<https://dl.dropbox.com/u/21172615/DSC03812.JPG>is a close-up of that 
'pill' at the top of the tube, showing the granular 
surface. For the getter to operate it must get warm/hot. The getter is also 
connected to the cathode which warms it up during operation. 
Here<https://dl.dropbox.com/u/21172615/DSC03813.JPG>is a close-up showing just 
this (apologies, it looked in focus on the 
camera). The thin wire is the end of the long cathode wire connected to the 
getter and stretched by bending that U-bracket.

If you want to activate the getter without the tube on...place the tubes in 
an oven. There are plastic parts inside so don't overdo it. Bake for 1h 
until crispy but not brown.
 
It is clear that your tubes have been left in storage for decades and 
therefore require cleaning of the impurities inside. The term for that is 
cathode cleaning by sputtering, or cathodic sputtering. Have a look at my 
post here for a method I use on IN-13s, same principles 
apply: 
https://groups.google.com/forum/?fromgroups=#!topic/neonixie-l/GAREG0tdVsI 
There are also a few comments on full-wave rectified or smoothed power 
supply.

You can easily clean the tubes with your setup. Just change the resistor to 
220 Ohms (to reduce the current to 200% of rated) and add an electrolytic 
tank capacitor after the rectifier to have a smooth DC supply. 47uF-470uF 
at 200-500V should do it. For a capacitor you can use the ones from an old 
PC power supply. Please use an appropriate voltage and be careful. Dont 
worry about the higher average voltage, the transistor will take care of 
that. Set your input to 5V and power on. Leave it for a couple of minutes. 
A 'dirty tube' will glow from some point on the bar and slowly fully 
illuminate. Others will be very close to the top and others at the top and 
very bright. Reduce the time for tubes that start at the top to say half. 
Once done safely discharge the capacitor.

Good luck!

Regards,
Alex

On Wednesday, March 13, 2013 4:39:45 PM UTC, rkvs wrote:
>
> I performed the test again after 10 minutes after posting the previous 
> message. I repeated Step #2 in Previous post again few times (using 150ohms 
> emitter resistance).
> Now, the tube glow reached 100% i think.
>
> I changed back emitter resistor to 330ohms and glow is now 95% of full 
> length. I'm wondering why it didnt work when I performed step #2 some time 
> back? Will 10 minutes gap inbetween do the trick???
>
>

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