> I see.. That taking a known volume could really work. But it is difficult to 
> use it directly in the tube (capillary with both ends open and a drop of 
> mercury), the mercury would evaporate during pumping messing the vacuum 
> system with vapours of mercury.. not good.

What you do is make a mercury trap.  Heat a spot of your narrow tubulation 
tubing and blow a bubble in it.  Tip the drop of mercury into the bubble and 
seal that tube to your vacuum system and the tube you're evacuating.  Now 
arrange to have the bubble sitting in a little cup of acetone cooled by dry 
ice.  The mercury will freeze, greatly lowering its vapor pressure.  After 
pumping, let the mercury re-melt, seal off the tube from your vacuum system, 
tip the droplet from the bubble into your tube, and then do the final seal-off 
of your tube.  Voilà!

- John

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