I restarted the server and the extension was added by default. Was there a need to do the compile?
No, I don't think so. You should only have to compile it if you're on a *nix machine. I'm not too familiar with Windows and IIS, but it sounds like the dll isn't getting loaded. Maybe check your error logs to see if IIS is telling you that. Also, check your extensions directory in the php.ini, and make sure it's pointing to where the .dll's are. There are some user comments on the mssql_connect() page of the manual which may help you out.
http://us4.php.net/manual/en/function.mssql-connect.php
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