Using "|Fobs|" extraction with Fullprof may provide
uncomplete lists of hkl for some high symmetry space groups .

For instance, using Im3 produces a .fou file in which one reflection
of the couples hkl/hlk disapear :

   0   1   1   11.30    0.15
   0   0   2   16.02    0.51
   1   1   2    5.00    0.77
   0   2   2   86.60    0.05
   0   1   3   66.52    0.06      _
   2   2   2  117.23    0.09
   1   2   3   71.34    0.04      _
   0   0   4  146.08    0.14

Although the .fou file in structure refinement mode is OK :

   0   1   1    2.83    0.04
   0   0   2    4.00    0.13
   1   1   2    1.25    0.19
   0   2   2   21.65    0.01
   0   1   3   22.18    0.02        -
   0   3   1    7.82    0.02        -
   2   2   2   29.30    0.02
   1   2   3   24.22    0.01        -
   1   3   2    7.02    0.01        -
   0   0   4   36.52    0.03


Anyway, since they exactly overlap, they should have the same
|F| if they are equipartitioned. So that I do not know if this is
intentional or not. However, depending on what you want to do with
such data, you should be aware of the hkl list incompleteness
in "|Fobs|" extraction mode.

Bug or not bug ?



Armel Le Bail - Universit� du Maine, Laboratoire des Fluorures,
CNRS ESA 6010, Av. O. Messiaen, 72085 Le Mans Cedex 9, France
http://www.cristal.org/

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