Dear Doinita (and others),
I'm assuming this is a GSAS question. The tic marks show the ideal position of the 
reflections according to Bragg's Law. The real peaks can be "out of position" for a 
variety of reasons including a non zero ZERO. Most usually for ordinary x-ray powder 
data the sample displacement is the usual systematic error. Refine "shft" - found in 
the profile function. A badly zeroed diffractometer will also show offsets. If the 
offset is small in the plots & the fit is OK then don't worry about the plot. If big 
then I'd look at the raw data to make sure the "START" value on the "BANK" record is 
correct.
Bob Von Dreele

________________________________

From: Doinita E Neiner [mailto:[EMAIL PROTECTED]
Sent: Fri 6/25/2004 4:57 PM
To: [EMAIL PROTECTED]


Hello,
 
Does anybody know how do you move the thick marks in the peaks position because though 
I have a good fit they are all shifted to the left. Shall I refine ZERO?
Anticipated thanks to any kind of suggestions.
 
Doinita

  • =20 Von Dreele, Robert B.
    • =20 Dr. John Faber

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