Hi,

It would be worth your while tracking down a copy of 

"Structure Determination from Powder Diffraction Data"
IUCr Monographs of Crystallography No. 13
Oxford University Press ISBN 0198500912

which contains roughly 300 pages dedicated to 
exactly the subject you are interested in.

With best regards,

Kenneth

PS: I trust that recommending a book nowadays does
    not qualify as commercial bias, just because it
    is not free!  Knowing this mailing list, one can 
    never be sure....

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