Actually any Extra-hold or Maximum-hold hair spray works fine. I use it not 
necessarily on the backload sample but on any spinning
sample even so the sample is horizontal. It's a bit tricky to put but it you keep at 
least 25-20 cm distance and do it slowly it
works fine.
Peter

-----Original Message-----
From: [EMAIL PROTECTED] [mailto:[EMAIL PROTECTED]
Sent: Thursday, September 09, 2004 10:24 AM
To: [EMAIL PROTECTED]



Try hair spray "Clynol". You may get it in good hair cutter shops.


Viele Gr��e
Wolfgang B�ttner


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-----Original Message-----
From: [EMAIL PROTECTED] [mailto:[EMAIL PROTECTED] Behalf
Of Andreas Leineweber
Sent: Thursday, September 09, 2004 3:57 PM
To: [EMAIL PROTECTED]



Dear all,

when powder samples are measured in reflection on back-loaded samples on
a theta-2theta diffractometer, there is always the danger that upon
sample spinning the powder can fall out of its cavity. As a solution I
tried a thin mylar foil, which, however, gives nasty background. Another
procedure may be a little bit of glue (e.g. dissolved in a solvent to
dillute it).
Has somebody some practical good experiences with certain types of glues
(influence on background, how much glue, which solvent) or does somebody
know some further tricks.
Thank you for your help
Andreas

PS. I am working with the Philips/Panalytical sample preparation equipment.

--
Dr. Andreas Leineweber
Max-Planck-Institut fuer Metallforschung
Heisenbergstrasse 3
70569 Stuttgart
Germany

Telephone: +49 (0)711 689 3365
Telefax: +49 (0)711 689 3312
[EMAIL PROTECTED]
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