(a) graininess or (b) preferred orientation. For (b) you may try if freeing of PO parameters improves refinement. For (a) just grind and pack your sample again and look if this eliminates your intensity problem.
best mg On 10 May 2005 at 22:05, �Jie Peng wrote: > > Dear all: > when i scan sample with x-ray,i foundthe intensity of one peak is > higher than it should be, i > don't know the reason, would you like to share the answer with > me?thanks > > > Jie Peng > College of Chemistry and chemical Engineering > Graduate School of the Chinese Academy of Sciences > 19(A) YuQuan Road > Beijing,100049 > China > phone:86-10-88256414 > > > Do You Yahoo!? > ������̫С���Ż������������ݣ� -- Miguel Gregorkiewitz Dip Scienze della Terra, Universit� via Laterino 8, I-53100 Siena, Europe fon +39'0577'233810 fax 233938 email [EMAIL PROTECTED]
