>I don't know how to generate a proper PCR file of the (La,Sr)MnO3 crystalline 
>powder

There are full instructions and examples of FullProf PCR files on our server: 
http://www.ill.fr/dif/Soft/fp/
In particular http://www.ill.fr/dif/Soft/fp/downloads/Docs/pcr_dat.zip contains 
a PCR file for LaMnO3
Alan.

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Dr Alan Hewat, ILL Grenoble, FRANCE<[EMAIL PROTECTED]>fax+33.476.20.76.48
+33.476.20.72.13 (.26 Mme Guillermet)  http://www.ill.fr/dif/people/hewat/
_____________________________________________________________

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