Dear rietvelders, I have carried out the single crystal resolution and the PXRD Le Bail refinement of a Metal Organic Framework. The compound crystalizes as needles and there is a clear in-plane preferred orientation along the c-axis. There is a mismatch between the single crystal and the Le Bail refinement data in the lattice parameter c. Could this mismatch be due to the preferred orientations?
Regards, Breogán Pato Doldán, Fundamental Chemistry Department. Faculty of Sciences. University of A Coruña Rúa da Fraga 10, 15008, A Coruña. Spain. Tel: +34 981167000 ext. 2061
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