Re: [Biofuel] Phosphoric acid

2006-10-29 Thread Mike Weaver
I get it at the hrdware store or the auto parts store

Bobby Clark wrote:

Anyone, can you answer my question?

Bobby



  

From: Bobby Clark [EMAIL PROTECTED]
Reply-To: biofuel@sustainablelists.org
To: biofuel@sustainablelists.org
Subject: [Biofuel]  Phosphoric acid
Date: Fri, 27 Oct 2006 10:44:31 -0400

I know now I can use phosphoric acid to separate out a crude glycerine
product. Where can I get phosphoric acid?

Also, for those who do the two stage acid/base process, where can I get
sulfuric acid? Down the road, I want to switch to this process, but I will
have to make a new processor, the sulfuric acid would probably eat the
plumbing in my current processor.

Thanks for all of your help!
Bobby

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Re: [Biofuel] Phosphoric acid

2006-10-29 Thread Bobby Clark

What product names are these acids under?

From: Mike Weaver [EMAIL PROTECTED]
Reply-To: biofuel@sustainablelists.org
To: biofuel@sustainablelists.org
Subject: Re: [Biofuel] Phosphoric acid
Date: Sun, 29 Oct 2006 15:56:05 -0500

I get it at the hrdware store or the auto parts store

Bobby Clark wrote:

 Anyone, can you answer my question?
 
 Bobby
 
 
 
 
 
 From: Bobby Clark [EMAIL PROTECTED]
 Reply-To: biofuel@sustainablelists.org
 To: biofuel@sustainablelists.org
 Subject: [Biofuel]  Phosphoric acid
 Date: Fri, 27 Oct 2006 10:44:31 -0400
 
 I know now I can use phosphoric acid to separate out a crude glycerine
 product. Where can I get phosphoric acid?
 
 Also, for those who do the two stage acid/base process, where can I get
 sulfuric acid? Down the road, I want to switch to this process, but I 
will
 have to make a new processor, the sulfuric acid would probably eat the
 plumbing in my current processor.
 
 Thanks for all of your help!
 Bobby
 
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 messages):
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Re: [Biofuel] Phosphoric acid

2006-10-28 Thread Bobby Clark
Anyone, can you answer my question?

Bobby



From: Bobby Clark [EMAIL PROTECTED]
Reply-To: biofuel@sustainablelists.org
To: biofuel@sustainablelists.org
Subject: [Biofuel]  Phosphoric acid
Date: Fri, 27 Oct 2006 10:44:31 -0400

I know now I can use phosphoric acid to separate out a crude glycerine
product. Where can I get phosphoric acid?

Also, for those who do the two stage acid/base process, where can I get
sulfuric acid? Down the road, I want to switch to this process, but I will
have to make a new processor, the sulfuric acid would probably eat the
plumbing in my current processor.

Thanks for all of your help!
Bobby

_
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Re: [Biofuel] Phosphoric acid

2006-10-28 Thread Ken Provost

On Oct 28, 2006, at 7:48 PM, Bobby Clark wrote:

 Anyone, can you answer my question?



Try a wholesaler of nursery chemicals -- fertilizers,
agricultural lime, etc.

-K

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[Biofuel] Phosphoric acid

2006-10-27 Thread Bobby Clark
I know now I can use phosphoric acid to separate out a crude glycerine 
product. Where can I get phosphoric acid?

Also, for those who do the two stage acid/base process, where can I get 
sulfuric acid? Down the road, I want to switch to this process, but I will 
have to make a new processor, the sulfuric acid would probably eat the 
plumbing in my current processor.

Thanks for all of your help!
Bobby

_
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[Biofuel] Phosphoric Acid in First Wash

2006-03-04 Thread Thomas Kelly
Todd,
 In a reply re: washing BD you suggested adding a small amount of 
phosphoric acid to the first wash. (0.20 ml 85% phosphoric acid/L of BD).
The results on a recent batch were impressive. I stir wash 76L (20 gal) 
batches. I usually go easy on the first wash and allow it to settle 
overnight. Second, third and fourth washes get buzzed pretty good. I allow 
2nd and 3rd to settle 2 - 3 hrs. and the 4th overnight.
 After adding 15 ml of 85% phosphoric acid to the first wash water, the 
mix separated cleanly in an hour or less.
I also achieved clear water after only three washes  ...  a first for me. 
Your suggestion saves me time, energy and water.
   Thanks,
Tom

- Original Message - 
From: Appal Energy [EMAIL PROTECTED]
To: Biofuel@sustainablelists.org
Sent: Thursday, February 23, 2006 7:11 PM
Subject: Re: [Biofuel] Compressed air wash
 Thomas,
 Bubble washing prolly won't condemn your fuel. But it does degrade it.
 Whether you use tiny bubbles... for a long duration or short bursts of 
compressed air, do you really think that there is less air contact with the 
fuel in the end run?

   On either wash type, you might try adding around 0.20 milliliters of 85% 
phosphoric acid to the wash water. This will allow more of the base soaps to 
come out in the first wash, reducing your overall wash  number/volume.

 Todd Swearingen

Thomas,
That's 0.20 ml per liter of fuel to be washed. Adjust as needed to bring 
the wash water to neutral, which means toy with it. Doing this in the first 
wash will yield remarkable improvements in any subsequent wash.
   Todd Swearingen



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Re: [biofuel] phosphoric acid in Foolproof method

2003-09-19 Thread Keith Addison

simonswb6 wrote:

In Aleks Foolproof method, step 18 recommends using %25 of the total
glycerine and mix with 10% phosphoric acid.  Can you use other types
of acids for this?  how about citric or sulfuric?  i have seen these
mentioned when doing the bubble wash?  Should you use the same acid
when doing the bubble wash as what was used in step 18?


 step 18 ***

18. For easier washing: Drain off the glycerine. Measure off 25% of
the total glycerine (including previously drained glycerine if you
followed step 15) and mix with 10 milliliters of 10% phosphoric acid
(H3PO4) for each litre of oil/fat processed. The mixing can be done
with a wooden spoon in a plastic container. Pour the acidified
glycerine back into the reactor and stir for 20 minutes, unheated.
Allow to settle for at least six hours and then drain the glycerine
fraction completely.

Both Step 15 and Step 18 are optional, not essential. You could try 
it without those steps first, if you have problems then include them.

Aleks advises:

A 10% citric solution should be fine, but avoid sulphuric acid, as 
it is too dissociated. You could also use HCl, also in a 10% 
solution.

I'd stick with the same acid in the bubblewash, but note that there's 
controversy over using any acid in the wash. See:
http://journeytoforever.org/biodiesel_bubblewash.html
Bubble washing - Washing problems - Using acid

There are several pages there on washing, all linked from this one 
above, I suggest you give them a thorough read and then make up your 
mind.

Note also that you don't have to wash biodiesel made by the Foolproof 
method any special way. That's how Aleks does it, and that's fine, 
but once it's settled and the by-product (glycerine) layer at the 
bottom removed, biodiesel is biodiesel and washing it is washing it, 
no matter what process you used. So you can decide for yourself 
what's best for you.

Best

Keith





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[biofuel] phosphoric acid in Foolproof method

2003-09-18 Thread simonswb6

In Aleks Foolproof method, step 18 recommends using %25 of the total 
glycerine and mix with 10% phosphoric acid.  Can you use other types 
of acids for this?  how about citric or sulfuric?  i have seen these 
mentioned when doing the bubble wash?  Should you use the same acid 
when doing the bubble wash as what was used in step 18?


 step 18 ***

18. For easier washing: Drain off the glycerine. Measure off 25% of 
the total glycerine (including previously drained glycerine if you 
followed step 15) and mix with 10 milliliters of 10% phosphoric acid 
(H3PO4) for each litre of oil/fat processed. The mixing can be done 
with a wooden spoon in a plastic container. Pour the acidified 
glycerine back into the reactor and stir for 20 minutes, unheated. 
Allow to settle for at least six hours and then drain the glycerine 
fraction completely.




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