Re: [volt-nuts] Calibration of voltage standards --- DIY switch/scannors

2015-02-15 Thread 张利民
Hi M K,

Sorry about that, I have posted a new thread on EEVBLOG with added photos.
http://www.eevblog.com/forum/projects/diy-low-thermal-emf-switchscanner-for-comparisons-of-voltage-and-resistor-stand/

lymex/bg2vo

-邮件原件-
发件人: volt-nuts [mailto:volt-nuts-boun...@febo.com] 代表 M K
发送时间: 2015年2月13日 14:45
收件人: volt-nuts@febo.com
主题: Re: [volt-nuts] Calibration of voltage standards

On 13/02/2015 01:40, 张利民 wrote:
 Dear Ken Peek,
 I designed a powerless automatic 2*4 low thermal EMF switch for 3458A, 
 34401A and 34420A(works also on my R6581T and 1281). It performs great and I 
 use it as my main comparison tool for 10V and 10k standards.
 http://bbs.38hot.net/thread-1186-1-1.html
 lymex/bg2vo

 -邮件原件-
 发件人: volt-nuts [mailto:volt-nuts-boun...@febo.com] 代表 Ken Peek
 发送时间: 2015年2月12日 1:35
 收件人: volt-nuts@febo.com
 主题: Re: [volt-nuts] Calibration of voltage standards

 I forgot to mention that I also own a PPM Inc. Model AVM-100 null meter.
 Works great on AC but I need to replace the NiCd batteries for it to
 work on batteries.  It has a 1uV scale, and it is a bit noisy on that
 scale.  I intend to modify it to get batter 1/f noise specs on the 1uV
 scale.

 Does anyone know where I can get [or how to make] a low-thermal-EMF
 switch [or relay]?  This would need to be a DPDT type to be able to
 reverse the connection to the meter.  Ideas?
Hi Lymex,

Great idea. I will have to spend some time looking over the google 
translate version of your text, as unfortunately it seems that here in 
the United Kingdom we cannot see any in line images from 38hot. I guess 
I would have to sign up to see them? And even the video of your box 
would not stream for me.


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Re: [volt-nuts] Calibration of voltage standards --- DIY switch/scannors

2015-02-15 Thread M K

On 16/02/2015 06:45, 张利民 wrote:

Hi M K,

Sorry about that, I have posted a new thread on EEVBLOG with added photos.
http://www.eevblog.com/forum/projects/diy-low-thermal-emf-switchscanner-for-comparisons-of-voltage-and-resistor-stand/

lymex/bg2vo


-邮件原件-
发件人: volt-nuts [mailto:volt-nuts-boun...@febo.com] 代表 M K
发送时间: 2015年2月13日 14:45
收件人: volt-nuts@febo.com
主题: Re: [volt-nuts] Calibration of voltage standards
On 13/02/2015 01:40, 张利民 wrote:

Dear Ken Peek,
I designed a powerless automatic 2*4 low thermal EMF switch for 3458A, 34401A 
and 34420A(works also on my R6581T and 1281). It performs great and I use it as 
my main comparison tool for 10V and 10k standards.
http://bbs.38hot.net/thread-1186-1-1.html

lymex/bg2vo

-邮件原件-
发件人: volt-nuts [mailto:volt-nuts-boun...@febo.com] 代表 Ken Peek
发送时间: 2015年2月12日 1:35
收件人: volt-nuts@febo.com
主题: Re: [volt-nuts] Calibration of voltage standards

I forgot to mention that I also own a PPM Inc. Model AVM-100 null meter.
Works great on AC but I need to replace the NiCd batteries for it to
work on batteries.  It has a 1uV scale, and it is a bit noisy on that
scale.  I intend to modify it to get batter 1/f noise specs on the 1uV
scale.

Does anyone know where I can get [or how to make] a low-thermal-EMF
switch [or relay]?  This would need to be a DPDT type to be able to
reverse the connection to the meter.  Ideas?

Hi Lymex,

Great idea. I will have to spend some time looking over the google
translate version of your text, as unfortunately it seems that here in
the United Kingdom we cannot see any in line images from 38hot. I guess
I would have to sign up to see them? And even the video of your box
would not stream for me.

Hi Lymex,

Amazing lab you have there. Thanks.

M K
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Re: [volt-nuts] Calibration of voltage standards

2015-02-12 Thread 张利民
Dear Ken Peek,
I designed a powerless automatic 2*4 low thermal EMF switch for 3458A, 34401A 
and 34420A(works also on my R6581T and 1281). It performs great and I use it as 
my main comparison tool for 10V and 10k standards.
http://bbs.38hot.net/thread-1186-1-1.html
lymex/bg2vo

-邮件原件-
发件人: volt-nuts [mailto:volt-nuts-boun...@febo.com] 代表 Ken Peek
发送时间: 2015年2月12日 1:35
收件人: volt-nuts@febo.com
主题: Re: [volt-nuts] Calibration of voltage standards

I forgot to mention that I also own a PPM Inc. Model AVM-100 null meter.
Works great on AC but I need to replace the NiCd batteries for it to
work on batteries.  It has a 1uV scale, and it is a bit noisy on that
scale.  I intend to modify it to get batter 1/f noise specs on the 1uV
scale.

Does anyone know where I can get [or how to make] a low-thermal-EMF
switch [or relay]?  This would need to be a DPDT type to be able to
reverse the connection to the meter.  Ideas?

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Re: [volt-nuts] Calibration of voltage standards

2015-02-11 Thread Todd Micallef
A Data Proof scanner seems to be the standard of some primary labs. They
don't show up often on the auction site.

This company makes one that fits the front of a 732B. I have never seen it
in use.

http://www.hpd-online.com/reversing_switch.php

There also appears to be a Guildline 9600 up for auction. It is misspelled
Guideline. I don't know the specs of that item, I have just noticed it has
been listed for a while.

Some of the Keithley instruments take low thermal cards, but they are not
reversible as far as I can tell. You might be able to do so with two
separate inputs. It is a Keithley 7168 nanovolt scanner card. If you can
get one, I am pretty sure you can plug it into a 7001/7002 scanner.

A home made switch might be cheaper if you can source some good low thermal
latching relays.

Todd

On Wed, Feb 11, 2015 at 12:35 PM, Ken Peek ken.p...@diligentminds.com
wrote:

 I forgot to mention that I also own a PPM Inc. Model AVM-100 null meter.
 Works great on AC but I need to replace the NiCd batteries for it to
 work on batteries.  It has a 1uV scale, and it is a bit noisy on that
 scale.  I intend to modify it to get batter 1/f noise specs on the 1uV
 scale.

 Does anyone know where I can get [or how to make] a low-thermal-EMF
 switch [or relay]?  This would need to be a DPDT type to be able to
 reverse the connection to the meter.  Ideas?

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Re: [volt-nuts] Calibration of voltage standards

2015-02-11 Thread Михаил
The most noiseless and stable nullmeter is any of the EM Electronics 
nanovoltmeter.
Even the oldest EM N1a I have, gives about 1 nV p-p noise and 1 pA input 
current.

Regards,
Mickle

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Re: [volt-nuts] Calibration of voltage standards

2015-02-11 Thread jeffhook

I have both the Keithley 155 and several Fluke 845AB's. 
I too prefer the Keithley 155 over the Fluke and I'm not a big fan of Keithley 
equipment. 
Jeff - KDØORH 

- Original Message -

From: R.Phillips phill...@btinternet.com 
To: volt-nuts@febo.com 
Sent: Wednesday, February 11, 2015 6:00:42 AM 
Subject: Re: [volt-nuts] Calibration of voltage standards 

I think I was the Keithley 155 owner that ask the question. Since then I 
have added an HP3245A to my equipment which I have set to 1.00 V DC, 
read by my in calibration HP3458A, and then compared by the Keithley 155 
against my Fluke 732A's 1.000 v output - this is showing a steady -1 uV on 
the 155's , 1 or 3uV range. I have replaced the batteries in the 155 with 9 
volt (6LF22/MB1604) batteries, works fine. I also have a Fluke 845AB which 
I would suggest is less stable. Best regards 

Roy Phillips. 


-Original Message- 
From: acb...@gmx.de 
Sent: Wednesday, February 11, 2015 10:00 AM 
To: volt-nuts@febo.com 
Subject: Re: [volt-nuts] Calibration of voltage standards 

for those interested, and for simplicity, wanted to add this from David 
which was in voltnuts in 2012. 


 
From: Charles P. Steinmetz charles_steinmetz at lavabit.com 
To: Discussion of precise voltage measurement volt-nuts at febo.com 
Sent: Saturday, 15 December 2012, 10:28 
Subject: Re: [volt-nuts] Fluke 335A versus HP 740B 

David wrote: 

 I have a Keithley 155 Null Detector how does that rate? 

The three usual suspects are the Fluke 845AB, the HP 419A, and Keithley 155. 
I have one of each, and they are all good meters. The received wisdom is 
that the Fluke is the one to have. However, in my view, the Keithley is the 
best of the bunch. It is a bonus if you find one with the rare 1554 AC 
power module (the 1554 mounts to the rear panel and allows AC operation -- 
otherwise, it is battery-only). 

The main problem today with the HP is that it uses impossible-to-find 
batteries. Not only are the original batteries unobtainable, I have yet to 
find a satisfactory replacement strategy. It also does not have a +/- 1 uV 
range, although I do not count that as a major fault since thermocouple 
noise in the measurement setup frequently prevents taking full advantage of 
the 1 uV range. 

The Fluke's batteries (sub-C NiCd cells) are readily replaced (though not 
inexpensively, if you get the best cells). Keithley used four, # 246 9 V 
carbon cells, which can easily be replaced with common 9 V alkalines or 9 V 
primary lithium cells that simply plug into the existing connectors. 

The HP and Fluke both use photocell choppers. Fluke published pre-release 
information indicating that they had designed a FET chopper for later 
production, but I have never seen an 845 with a FET chopper or a schematic 
of the FET chopper. (Does anyone here have either?) The Keithley was 
designed with a MOSFET chopper from the start. 

Not only is the Keithley the most modern design and the most likely to 
remain reliable, it also performs the best in my lab. I have had fewer 
ground loop and shielding problems with it than with the Fluke, and it has 
less noise and less drift. It is not enough better that most people should 
sell their Fluke to get a Keithley just for the performance difference 
(reliability may be another story), but -- IME -- it does perform better. 

They are all good meters, but IMO the Keithley is the best of the three. If 
I had only one, that is the one I'd want. 

Best regards, 

Charles 

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Re: [volt-nuts] Calibration of voltage standards

2015-02-11 Thread Charles Steinmetz

Jeff wrote:


I have both the Keithley 155 and several Fluke 845AB's.
I too prefer the Keithley 155 over the Fluke and I'm not a big fan 
of Keithley equipment.


There's a 155 with a halfway reasonable BIN on ebay right now.  It 
has the rare and (IMO) desirable 1554 AC power supply.  I doubt it 
will be there long.  (I have no connection to or knowledge of the seller.)


There are manuals on ko4bb.com.

Best regards,

Charles



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Re: [volt-nuts] Calibration of voltage standards

2015-02-11 Thread acbern
the 3458A is very well suited as a nullmeter (there e.g. also is an appnote 
from Fluke on this). I have checked this against other meters such as the e.g. 
the keithley 155 and 34420A, and for my setup (Fluke 732A, Datron 4910 and 
others) I have the least problems with noise, common mode issues and so.
The nullmeter method should only be used when the DUT is adjusted. ie., low 
voltages differnces of a few mV should not be measured, the accuracy is, at 
least formally, not specified there sufficiently precise.
The second method frequently used and that I am using most of the time (since I 
do not adjust references, especially the 732A is known to potentially increase 
its drift thereafter, the 4910 uses digital adjustment, so there it would be 
ok) is to measure the absolute voltage of both standards with a 3458A and 
reference the DUT to the standard. This can be done because of the excellent 
linearity of the 3458A. If I remember correctly the accuracy related to the 
standard is in the 0,1ppm range at 10V.





 Gesendet: Mittwoch, 11. Februar 2015 um 08:36 Uhr
 Von: Chuck Harris cfhar...@erols.com
 An: Discussion of precise voltage measurement volt-nuts@febo.com
 Betreff: Re: [volt-nuts] Calibration of voltage standards

 To do a comparison of the sort you are asking about, the
 sensitivity of the null meter is much more important than
 its ultimate accuracy.
 
 So, neither of your meters is really the right meter to
 use for this task.  What you want is called a null meter,
 and is generally sensitive to the microvolt region.
 
 -Chuck Harris
 
 Ken Peek wrote:
  Hi Group,
 
  I have heard of a few different ways to measure one 10V voltage standard
  against another 10V voltage standard.
 
  Assume we have two 10V voltage standards.  One is calibrated, the other
  not only needs to be calibrated, but probably adjusted.  For the sake of
  simplicity, let's say the two standards are Fluke 732B's.
 
  I *think* the best way is to connect the two units' (-) terminals
  together, then connect a calibrated meter in between the (+) terminals,
  and measure the difference.  I have also heard that to remove thermal
  EMFs, you should use a low-thermal-EMF DPDT switch or a low-thermal-EMF
  relay to reverse the connections on the DMM, so you can take the reading
  forward and reversed, then split the difference.  There is the
  possibility to introduce thermal-EMF errors from the switch/relay as
  well, so I'm wondering if this is a good idea.  This sort of makes sense
  to me, but I'm not a metrologist, so I would like to hear what others in
  this group think about this.
 
  So, just what is the proper way to accomplish this task?
 
  BTW-- I have an Agilent 34420A and an HP 3458A, which would be the
  better instrument for this task?
 
  Best Regards,
  Ken Peek
  =
 
 
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[volt-nuts] Calibration of voltage standards

2015-02-11 Thread frank . stellmach
Hello Ken,
 
generally, the difference (bridge) method is always the most sensitive and 
precise one.
 
Thermal voltages and amplifier noise pose a lower limit to the achievable 
precisison.
 
About 10nV may be achieved at best, even in metrological environment.. 
 
That's the reason, why the 1e-18 stability / uncertainty between two JJ arrays 
against each other, (superconducting environment), can be transferred to the 
analogue world to 1e-9 uncertainty only (10nV / 10V).
 
 
 
To compare two 10V standards, an uncertainty of only 1µV is required, as this 
will yield 0.1ppm uncertainty of the 10V transfer - totally sufficient in 
practical terms. Btw.: the unit 'Volt' currently is 0.2ppm uncertain only in 
the SI system. (Will probably change in 2018!) 
 
Good low thermo voltage cables are required, maybe also a low thermal switch.
 
 
Therefore, both of your instruments can of course successfully and easily 
compare and null these two 10V references, and would also be able to give a 
precise difference reading, so to assign the DUT a calibrated standrad value, 
differing from a clean 10.00V.
 
The 34420 is better suited, as it has better noise and higher resolution 
(100pV).
This instrument can even be used to make a transfer from a JJ array primary 
standard to a 732B secondary standard.
 
Rem.: There's a good application note from FLUKE, where they promote their 
8508A reference multimeter as good replacement for differential meters like 
their famous 845A...
 
 
 
The 3458A on the other hand is capable of making ultra precise absolute value 
transfers (better than the 720A), i.e. you may measure the absolute value of 
your 732B reference standard, and then measure the DUT 732B also on the 3458A, 
to compare their values in absolute terms.
 
This transfer can also be made uncertain to  0.1ppm, good thermal connections 
and maybe thermo voltage cancellation provided.
This again is equivalent to  1µV level uncertainty, which is not so difficult 
to achieve.
 
Frank


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[volt-nuts] Calibration of voltage standards

2015-02-11 Thread frank . stellmach
One further remark:
 
These high resolution, low noise DMMs, as 3458A, 8508A, 34420A all are capable 
to replace the 845A null voltmeter!
All have higher sensitivity, and at least same or better noise performance. 
(see also the FLUKE AN)
 
Especially in this application, i.e. low impedance sources, the bias current 
plays no role.
 
But also in the usual, higher impedance applications, like Wheatstone Bridges, 
where the 845A was intended for, the modern instruments can also be used 
without any problem.
 
Their bias currents are all specified to be  20..50pA, and may be taken into 
account in the uncertainty budget.
In practisey, my own 3458A  shows  2pA only.
 
In contrast to that, the 845A was never (!) specified for bias current.
Fluke only claimed something like  10^12 Ohm when nulled to  10µV, or so.
 
 
The 845A contains an optical chopper, but I'm not convinced that this design 
really is superior to modern FET choppers, which can be found in the 
instruments mentioned.
 
Maybe, volt-nuts owners of an 845A can really determine its leakage / bias 
current.
 
Maybe also, that this mystified instrument really is not as good in this 
aspect, as everybody assumed for the past decades.
 
Frank


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Re: [volt-nuts] Calibration of voltage standards

2015-02-11 Thread wb6bnq

To amplify Chuck's point,

The only meter worth considering, if you are going to get one, is the 
FLUKE 845.  Preferably, the battery operated version which has a higher 
isolation leakage resistance.  However, the 110

volt rack mount model would do just as equally.

BillWB6BNQ


Chuck Harris wrote:


To do a comparison of the sort you are asking about, the
sensitivity of the null meter is much more important than
its ultimate accuracy.

So, neither of your meters is really the right meter to
use for this task.  What you want is called a null meter,
and is generally sensitive to the microvolt region.

-Chuck Harris

Ken Peek wrote:


Hi Group,

I have heard of a few different ways to measure one 10V voltage standard
against another 10V voltage standard.

Assume we have two 10V voltage standards.  One is calibrated, the other
not only needs to be calibrated, but probably adjusted.  For the sake of
simplicity, let's say the two standards are Fluke 732B's.

I *think* the best way is to connect the two units' (-) terminals
together, then connect a calibrated meter in between the (+) terminals,
and measure the difference.  I have also heard that to remove thermal
EMFs, you should use a low-thermal-EMF DPDT switch or a low-thermal-EMF
relay to reverse the connections on the DMM, so you can take the reading
forward and reversed, then split the difference.  There is the
possibility to introduce thermal-EMF errors from the switch/relay as
well, so I'm wondering if this is a good idea.  This sort of makes sense
to me, but I'm not a metrologist, so I would like to hear what others in
this group think about this.

So, just what is the proper way to accomplish this task?

BTW-- I have an Agilent 34420A and an HP 3458A, which would be the
better instrument for this task?

Best Regards,
Ken Peek
=


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Re: [volt-nuts] Calibration of voltage standards

2015-02-11 Thread R.Phillips
I think I was the Keithley 155 owner that ask the question.  Since then I 
have added an HP3245A to my equipment which I have set to 1.00 V DC, 
read by my in calibration HP3458A, and then compared by the Keithley 155 
against my Fluke 732A's 1.000 v output - this is showing a steady -1 uV on 
the 155's , 1 or 3uV range. I have replaced the batteries in the 155 with 9 
volt (6LF22/MB1604) batteries, works fine.   I also have a Fluke 845AB which 
I would suggest is less stable. Best regards


Roy Phillips.


-Original Message- 
From: acb...@gmx.de

Sent: Wednesday, February 11, 2015 10:00 AM
To: volt-nuts@febo.com
Subject: Re: [volt-nuts] Calibration of voltage standards

for those interested, and for simplicity, wanted to add this from David 
which was in voltnuts in 2012.




From: Charles P. Steinmetz charles_steinmetz at lavabit.com
To: Discussion of precise voltage measurement volt-nuts at febo.com
Sent: Saturday, 15 December 2012, 10:28
Subject: Re: [volt-nuts] Fluke 335A versus HP 740B

David wrote:


I have a Keithley 155 Null Detector how does that rate?


The three usual suspects are the Fluke 845AB, the HP 419A, and Keithley 155. 
I have one of each, and they are all good meters.  The received wisdom is 
that the Fluke is the one to have.  However, in my view, the Keithley is the 
best of the bunch.  It is a bonus if you find one with the rare 1554 AC 
power module (the 1554 mounts to the rear panel and allows AC operation --  
otherwise, it is battery-only).


The main problem today with the HP is that it uses impossible-to-find 
batteries.  Not only are the original batteries unobtainable, I have yet to 
find a satisfactory replacement strategy.  It also does not have a +/- 1 uV 
range, although I do not count that as a major fault since thermocouple 
noise in the measurement setup frequently prevents taking full advantage of 
the 1 uV range.


The Fluke's batteries (sub-C NiCd cells) are readily replaced (though not 
inexpensively, if you get the best cells).  Keithley used four, # 246 9 V 
carbon cells, which can easily be replaced with common 9 V alkalines or 9 V 
primary lithium cells that simply plug into the existing connectors.


The HP and Fluke both use photocell choppers.  Fluke published pre-release 
information indicating that they had designed a FET chopper for later 
production, but I have never seen an 845 with a FET chopper or a schematic 
of the FET chopper.  (Does anyone here have either?)  The Keithley was 
designed with a MOSFET chopper from the start.


Not only is the Keithley the most modern design and the most likely to 
remain reliable, it also performs the best in my lab.  I have had fewer 
ground loop and shielding problems with it than with the Fluke, and it has 
less noise and less drift.  It is not enough better that most people should 
sell their Fluke to get a Keithley just for the performance difference 
(reliability may be another story), but -- IME -- it does perform better.


They are all good meters, but IMO the Keithley is the best of the three.  If 
I had only one, that is the one I'd want.


Best regards,

Charles



Gesendet: Mittwoch, 11. Februar 2015 um 08:55 Uhr
Von: wb6bnq wb6...@cox.net
An: Discussion of precise voltage measurement volt-nuts@febo.com
Betreff: Re: [volt-nuts] Calibration of voltage standards

To amplify Chuck's point,

The only meter worth considering, if you are going to get one, is the
FLUKE 845.  Preferably, the battery operated version which has a higher
isolation leakage resistance.  However, the 110
volt rack mount model would do just as equally.

BillWB6BNQ


Chuck Harris wrote:

 To do a comparison of the sort you are asking about, the
 sensitivity of the null meter is much more important than
 its ultimate accuracy.

 So, neither of your meters is really the right meter to
 use for this task.  What you want is called a null meter,
 and is generally sensitive to the microvolt region.

 -Chuck Harris

 Ken Peek wrote:

 Hi Group,

 I have heard of a few different ways to measure one 10V voltage 
 standard

 against another 10V voltage standard.

 Assume we have two 10V voltage standards.  One is calibrated, the other
 not only needs to be calibrated, but probably adjusted.  For the sake 
 of

 simplicity, let's say the two standards are Fluke 732B's.

 I *think* the best way is to connect the two units' (-) terminals
 together, then connect a calibrated meter in between the (+) terminals,
 and measure the difference.  I have also heard that to remove thermal
 EMFs, you should use a low-thermal-EMF DPDT switch or a low-thermal-EMF
 relay to reverse the connections on the DMM, so you can take the 
 reading

 forward and reversed, then split the difference.  There is the
 possibility to introduce thermal-EMF errors from the switch/relay as
 well, so I'm wondering if this is a good idea.  This sort of makes 
 sense
 to me, but I'm not a metrologist, so I would like to hear what

[volt-nuts] Calibration of voltage standards

2015-02-10 Thread Ken Peek
Hi Group,

I have heard of a few different ways to measure one 10V voltage standard
against another 10V voltage standard.

Assume we have two 10V voltage standards.  One is calibrated, the other
not only needs to be calibrated, but probably adjusted.  For the sake of
simplicity, let's say the two standards are Fluke 732B's.

I *think* the best way is to connect the two units' (-) terminals
together, then connect a calibrated meter in between the (+) terminals,
and measure the difference.  I have also heard that to remove thermal
EMFs, you should use a low-thermal-EMF DPDT switch or a low-thermal-EMF
relay to reverse the connections on the DMM, so you can take the reading
forward and reversed, then split the difference.  There is the
possibility to introduce thermal-EMF errors from the switch/relay as
well, so I'm wondering if this is a good idea.  This sort of makes sense
to me, but I'm not a metrologist, so I would like to hear what others in
this group think about this.

So, just what is the proper way to accomplish this task?

BTW-- I have an Agilent 34420A and an HP 3458A, which would be the
better instrument for this task?

Best Regards,
Ken Peek
=


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