Doyoub's question is a common enough one that I added a section to the Athena user manual:

http://bruceravel.github.io/demeter/documents/Athena/bkg/short.html

My answer to Doyoub's question is much the same as Matt's.

B

On 03/17/2017 09:18 AM, Matt Newville wrote:
Dear Doyoub,



On Thu, Mar 16, 2017 at 10:59 PM, 김도엽(신소재공학과)
<mdyk...@postech.ac.kr <mailto:mdyk...@postech.ac.kr>> wrote:

    Hello



    I'm a graduate student at POSTECH in Korea.

    Currently, I obtained XANES spectra over a narrow energy range and
    looked through the Athena manual


    But, I'm kind of lost as to how exactly I'm supposed to normalize
    raw data

    which only has XANES spectra.


    It would be very generous of you if you help me figure this out


It's hard for us to answer questions that are so vague.

Generally, it is recommended to collect XANES spectra out to at least
100 eV (and better 300 eV) above the edge in order to get a decent
normalization.  Well, for "normal" hard X-ray spectra: for edges below
about 3000 eV, you can often get by with less energy range.

If you don't have that, it is sometimes OK to pick an energy as far
above the edge as possible and pick an edge step so that all the spectra
is 1.0 at that energy.  That is definitely prone to systematic biases in
normalization.   Furthermore, if your data is particularly noisy, it can
add a lot of variation in the normalization to use just a single energy.

Which just brings me back to the original point: it's hard to say in
general how to best handle XANES with a short energy range.

--Matt


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--
 Bruce Ravel  ------------------------------------ bra...@bnl.gov

 National Institute of Standards and Technology
 Synchrotron Science Group at NSLS-II
 Building 743, Room 114
 Upton NY, 11973

 Homepage:    http://bruceravel.github.io/home/
 Software:    https://github.com/bruceravel
 Demeter:     http://bruceravel.github.io/demeter/
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