Re: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater

2019-07-26 Thread Payzant, Andrew
We always used to spot weld the T/C to the bottom of the strip. A big challenge is to avoid pickup of voltage from the strip (which is resistively heated) by the T/C – this can lead to false temperature indications, sometimes huge! I strongly recommend verification of the temperature by some

Re: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater

2019-07-26 Thread Payzant, Andrew
I agree with Tim. HT stages such as Anton Paar’s XRK900 provide excellent temperature control and stability across a range of atmospheres. One advantage that strip heaters still have is in rapid heating and cooling. A --- Dr.

RE: [EXTERNAL] Mounting Sample on High Temperature XRD Ribbon Heater

2019-07-26 Thread Timothy Hyde
Blaise, Andrew, below correctly summarises the issues with strip heaters, and as Julian mentions, even if you can get them working satisfactorily they are essentially rather expensive consumables. While for you not an immediate solution, for the reasons outlined by Andrew and Julian, we moved