Re: Is it really preferred orientation problem?

2004-03-15 Thread Alan Hewat
At 10:02 15/03/2004, Armel Le Bail wrote: The preferred orientation (PO) problem is recurrent at the rietveld_l. This is normal since PO is one of the biggest problem... Given that a neutron experiment is very expensive, some recommendations should be inside of the powder neutron... Armel is righ

Re: Is it really preferred orientation problem?

2004-03-15 Thread Armel Le Bail
> Like Rp, Rwp, Chi2, RB are respectively from 3.96, 5.33, 2.68, 5.80 > to 3.35, 4.42, 1.85, 3.07. This should pass a test of statistical significance. The preferred orientation (PO) problem is recurrent at the rietveld_l. This is normal since PO is one o

Re: Is it really preferred orientation problem?

2004-03-15 Thread Jon Wright
zhijian fan wrote: *> Like Rp, Rwp, Chi2, RB are respectively from 3.96, 5.33, 2.68, 5.80 > to 3.35, 4.42, 1.85, 3.07. This should pass a test of statistical significance. * I made a hypothesis testing. H0: It needs not PO correction. The model with PO correction: G1=sum[wi

Re: Is it really preferred orientation problem?

2004-03-14 Thread zhijian fan
Title: Message Dear all, When dealing with pref. orientation (PO), like with structure, it should make physical sense. For example if you have needle-like crystals pref. orientation coefficient should be greater than 1 (not less as in your case) and PO axis should be aligned

Is it really preferred orientation problem?

2004-03-06 Thread zavalij
---From: zhijian fan [mailto:[EMAIL PROTECTED] Sent: Thursday, March 04, 2004 3:40 PMTo: [EMAIL PROTECTED]Subject: Is it really preferred orientation problem? Dear all, I was making a Rietvled analysis of a neutron powder diffraction patters from intermetallic compound LaNi4.25Al0.75

Re: Is it really preferred orientation problem?

2004-03-05 Thread Jon Wright
> Like Rp, Rwp, Chi2, RB are respectively from 3.96, 5.33, 2.68, 5.80 > to 3.35, 4.42, 1.85, 3.07. This should pass a test of statistical significance. That does not mean it really is preferred orientation, but if it is not preferred orientation, then you

Is it really preferred orientation problem?

2004-03-04 Thread zhijian fan
Dear all, I was making a Rietvled analysis of a neutron powder diffraction patters from intermetallic compound LaNi4.25Al0.75. If not using preferred orientation correction, the agreement indices are a little higher than those when using it. Like Rp, Rwp, Chi2, RB are respectively from