with some materials, I observed powder diffraction patterns (Bragg-Brentano,
X'pert) which
show a broad negative peak around 5-6º(2th), instead of the smoothly descending
intensity
coming from the primary beam.
Did some of you observe the same phenomenon, and has this been dealt with
anywhere
refinement, as they must be fitted by a modulated background model...
Reinhard
Am 21/11/2013 12:32, schrieb gre...@unisi.it:
with some materials, I observed powder diffraction patterns (Bragg-Brentano,
X'pert) which
show a broad negative peak around 5-6º(2th), instead of the smoothly descending