Re: sealing capillary in a glove box

2023-02-03 Thread miguel gregorkiewitz 
Dear Angeles,

A couple of minutes ago I sent you the zip file containg the documents of
our manipulator to seal capillaries etc.

Let me know if you have any.problems!

Best

Miguel

El vie, 3 feb. 2023 15:39, miguel gregorkiewitz 
escribió:

> Dear Angeles,
>
> Here i send you the zip file containing the relevant documents. Please let
> me know if you have any problems.
>
> Good luck!
>
> Miguel
>
> El jue, 2 feb. 2023 9:30, M. Angeles Gomez de la Torre 
> escribió:
>
>> Dear Miguel,
>> I am Angeles G. De la Torre (
>> https://sites.google.com/view/angelesgdelatorre/ ).
>> I am interested in this discussion about sealing of capillaries. Could
>> you share with me the zip file you mentioned in the Rietveld list?
>> Thank in advance for your time.
>>
>> Best
>> Angeles
>>
>> l 02/02/2023 a las 8:35, miguel gregorkiewitz escribió:
>>
>> Dear Dharmalingam,
>>
>> A couple of minutes ago I sent you a zip file containg the documents of
>> our manipulator to seal capillaries etc.
>>
>> Let me know if you have any.problems!
>>
>> Best
>>
>> Miguel
>>
>> El jue, 2 feb. 2023 8:30, miguel gregorkiewitz 
>> escribió:
>>
>>> Dear Dharmalingam,
>>>
>>> Here i send you a zip file containing the relevant documents. Please let
>>> me know if you have any problems.
>>>
>>> Good luck!
>>>
>>> Miguel
>>>
>>> El mié, 1 feb. 2023 9:22, Dharmalingam Prabhakaran <
>>> dharmalingam.prabhaka...@physics.ox.ac.uk> escribió:
>>>
 Dear Miguel,


 We have an organic air-sensitive sample and struggling to measure it in
 our single crystal XRD machine.
 Could you please send me your capillary sealing details?

 Thank you very much.

 Best Wishes
 Prabhakaran



 _
 Dr. D. Prabhakaran
 Clarendon Laboratory
 University of Oxford
 Oxford OX1 3PU
 United Kingdom




>> ++
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>> 
>> Send commands to   eg: HELP as the subject 
>> with no body text
>> The Rietveld_L list archive is on 
>> http://www.mail-archive.com/rietveld_l@ill.fr/
>> ++
>>
>>
>>
>> --
>> Dr. M. Ángeles Gómez de la Torre
>> Catedrática de Universidad
>> Dpt. Química Inorgánica, Cristalografía y Mineralogía
>> Facultad de Ciencias, Universidad de Málaga
>> Campus de Teatinos 29010 Málaga
>> Telf: +34 952131877
>> Fax: +34 952131870 / +34 
>> 952132000https://sites.google.com/view/angelesgdelatorre/https://sites.google.com/view/cementscience-uma/home
>> Skype: angelesgt
>>
>>
++
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++

Re: sealing capillary in a glove box

2023-02-01 Thread miguel gregorkiewitz 
Dear Dharmalingam,

A couple of minutes ago I sent you a zip file containg the documents of our
manipulator to seal capillaries etc.

Let me know if you have any.problems!

Best

Miguel

El jue, 2 feb. 2023 8:30, miguel gregorkiewitz 
escribió:

> Dear Dharmalingam,
>
> Here i send you a zip file containing the relevant documents. Please let
> me know if you have any problems.
>
> Good luck!
>
> Miguel
>
> El mié, 1 feb. 2023 9:22, Dharmalingam Prabhakaran <
> dharmalingam.prabhaka...@physics.ox.ac.uk> escribió:
>
>> Dear Miguel,
>>
>>
>> We have an organic air-sensitive sample and struggling to measure it in
>> our single crystal XRD machine.
>> Could you please send me your capillary sealing details?
>>
>> Thank you very much.
>>
>> Best Wishes
>> Prabhakaran
>>
>>
>>
>> _
>> Dr. D. Prabhakaran
>> Clarendon Laboratory
>> University of Oxford
>> Oxford OX1 3PU
>> United Kingdom
>>
>>
>>
>>
++
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Send commands to  eg: HELP as the subject with no body text
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++

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz 
Dear Mirela,

 if you are working with quartz capillaries, i would use Pt for the
filament. The plastic parts on the connectors can be removed. I actually
did this already in the basic design. Let me know if you can reach the
necessary temperature!

Best

Miguel


El mié, 1 feb. 2023 8:18, miguel gregorkiewitz 
escribió:

> Dear Mirela,
>
> A couple of minutes ago I sent you a zip file containg the documents of
> our manipulator to seal capillaries etc.
>
> Let me know if you have any.problems!
>
> Best
>
> Miguel
>
> El mié, 1 feb. 2023 0:22, mirela dragomir 
> escribió:
>
>> Dear Miguel,
>>
>> I'm also intrigued by your setup and would like to learn more. Currently,
>> we are sealing our quartz capillaries outside of the glove box.
>>
>> Thank you and best regards,
>>
>> Mirela
>>
>> 
>>
>> Asst. Prof. Mirela Dragomir
>>
>> Electronic Ceramics Department, K5
>>
>> http://www-k5.ijs.si/
>>
>> Jožef Stefan Institute
>>
>> Jamova cesta 39,  1000 Ljubljana, Slovenia
>>
>> Associate Editor, Acta Chimica Slovenica
>>
>> https://acta.chem-soc.si/
>>
>> E-mail: mirela.drago...@ijs.si
>>
>> Web: http://eccl.ijs.si/
>>
>> Phone: +386 1 477 3512
>>
>>
>>
>> On Monday, January 30, 2023 at 01:10:41 PM GMT+1, miguel gregorkiewitz <
>> gregorm...@gmail.com> wrote:
>>
>>
>> I constructed an electrical heater which is used with a tunable power
>> supply and a microscope if possible. Let me know if you like to have
>> details of the design!
>>
>> Miguel
>>
>>
>> El lun, 30 ene. 2023 12:01, francois Goutenoire <
>> francois.gouteno...@univ-lemans.fr> escribió:
>>
>> Dear Rietveld users,
>>
>> We are currently working with some very hygroscopic compounds in
>> capillaries.
>>
>> These capillaries are fill in a glove box (N2).
>>
>> How can we sealed these capillaries (borosilicate) in the glove box ?
>>
>> Best wishes, François
>>
>> --
>> *
>> Pr. Francois GOUTENOIRE
>> e-mail: francois.gouteno...@univ-lemans.fr
>> Tel: 02.43.83.33.54
>> FAX: 02.43.83.35.06
>> Institut des Molécules et des Matériaux du Mans
>> IMMM - UMR CNRS 6283
>> Elaboration et Caracterisation des Composés Cristalisés (E3C)
>> Université du Maine - Avenue Olivier Messiaen
>> F-72085 Le Mans Cedex 9
>> FRANCE
>> *
>> Formation Rietveld 
>> CNRShttps://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135
>> Formation EDX CNRShttps://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135
>> Formation SAXS et Réflectivités pour couches minces et matériaux 
>> nanostructurés.https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135
>> Bibliographiehttps://scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=titlehttps://orcid.org/-0001-5339-3002
>>
>> ++
>> Please do NOT attach files to the whole list > >
>> Send commands to  eg: HELP as the subject with no body
>> text
>> The Rietveld_L list archive is on
>> http://www.mail-archive.com/rietveld_l@ill.fr/
>> ++
>>
>> ++
>> Please do NOT attach files to the whole list <
>> alan.he...@neutronoptics.com>
>> Send commands to  eg: HELP as the subject with no body
>> text
>> The Rietveld_L list archive is on
>> http://www.mail-archive.com/rietveld_l@ill.fr/
>> ++
>>
>>
++
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Send commands to  eg: HELP as the subject with no body text
The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/
++

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz 
Dear Mirela,

A couple of minutes ago I sent you a zip file containg the documents of our
manipulator to seal capillaries etc.

Let me know if you have any.problems!

Best

Miguel

El mié, 1 feb. 2023 0:22, mirela dragomir 
escribió:

> Dear Miguel,
>
> I'm also intrigued by your setup and would like to learn more. Currently,
> we are sealing our quartz capillaries outside of the glove box.
>
> Thank you and best regards,
>
> Mirela
>
> 
>
> Asst. Prof. Mirela Dragomir
>
> Electronic Ceramics Department, K5
>
> http://www-k5.ijs.si/
>
> Jožef Stefan Institute
>
> Jamova cesta 39,  1000 Ljubljana, Slovenia
>
> Associate Editor, Acta Chimica Slovenica
>
> https://acta.chem-soc.si/
>
> E-mail: mirela.drago...@ijs.si
>
> Web: http://eccl.ijs.si/
>
> Phone: +386 1 477 3512
>
>
>
> On Monday, January 30, 2023 at 01:10:41 PM GMT+1, miguel gregorkiewitz <
> gregorm...@gmail.com> wrote:
>
>
> I constructed an electrical heater which is used with a tunable power
> supply and a microscope if possible. Let me know if you like to have
> details of the design!
>
> Miguel
>
>
> El lun, 30 ene. 2023 12:01, francois Goutenoire <
> francois.gouteno...@univ-lemans.fr> escribió:
>
> Dear Rietveld users,
>
> We are currently working with some very hygroscopic compounds in
> capillaries.
>
> These capillaries are fill in a glove box (N2).
>
> How can we sealed these capillaries (borosilicate) in the glove box ?
>
> Best wishes, François
>
> --
> *
> Pr. Francois GOUTENOIRE
> e-mail: francois.gouteno...@univ-lemans.fr
> Tel: 02.43.83.33.54
> FAX: 02.43.83.35.06
> Institut des Molécules et des Matériaux du Mans
> IMMM - UMR CNRS 6283
> Elaboration et Caracterisation des Composés Cristalisés (E3C)
> Université du Maine - Avenue Olivier Messiaen
> F-72085 Le Mans Cedex 9
> FRANCE
> *
> Formation Rietveld 
> CNRShttps://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135
> Formation EDX CNRShttps://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135
> Formation SAXS et Réflectivités pour couches minces et matériaux 
> nanostructurés.https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135
> Bibliographiehttps://scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=titlehttps://orcid.org/-0001-5339-3002
>
> ++
> Please do NOT attach files to the whole list  >
> Send commands to  eg: HELP as the subject with no body
> text
> The Rietveld_L list archive is on
> http://www.mail-archive.com/rietveld_l@ill.fr/
> ++
>
> ++
> Please do NOT attach files to the whole list  >
> Send commands to  eg: HELP as the subject with no body
> text
> The Rietveld_L list archive is on
> http://www.mail-archive.com/rietveld_l@ill.fr/
> ++
>
>
++
Please do NOT attach files to the whole list 
Send commands to  eg: HELP as the subject with no body text
The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/
++

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz 
Dear Sergey,

A couple of minutes ago I sent you a zip file containg the documents of our
manipulator to seal capillaries etc.

Let me know if you have any.problems!

Best

Miguel

El mar, 31 ene. 2023 23:47, Sergey Ushakov  escribió:

> Hi Miguel,
>
> I would appreciate learning about your design as well.
> I was thinking to use TIG welder for this, but it probably overkill ;)
>
> Sincerely,
> Sergey
>
>
> Sergey V. Ushakov
>
> Associate Research Professor
> Center for Materials of the Universe
> School of Molecular Sciences
> Arizona State University
> 551 E. University Dr. PSG-106
> Tempe, AZ  85287-1604
>
>
> On Tue, Jan 31, 2023 at 3:26 PM miguel gregorkiewitz 
> wrote:
>
>> Dear Peter,
>>
>> A couple of minutes ago I sent you a zip file containg the documents of
>> our manipulator to seal capillaries etc.
>>
>> Let me know if you have any.problems!
>>
>> Best
>>
>> Miguel
>>
>> El lun, 30 ene. 2023 19:19, Khalifah, Peter  escribió:
>>
>>> Hello Miguel,
>>>
>>>
>>>
>>> I’d love to learn more about your design if you don’t mind sharing.  We
>>> have been thinking for a while about doing something like this.
>>>
>>>
>>>
>>> Best wishes,
>>>
>>>
>>>
>>> Peter
>>>
>>> Professor  Chemist
>>> Dept. of Chemistry Dept. of Chemistry
>>> Stony Brook University Brookhaven National Laboratory
>>> Stony Brook, NY 11794-3400 Upton, NY 11973-5000
>>>
>>> Office: 447 Grad. ChemistryOffice: Bldg 555, Rm 340
>>> Phone: (631)632-7796   Phone: (631)344-7689
>>> Fax: (631)632-7960 Fax: (631)344-5815
>>>
>>> Web page: https://sites.google.com/a/stonybrook.edu/pgk/home
>>> <https://urldefense.proofpoint.com/v2/url?u=https-3A__sites.google.com_a_stonybrook.edu_pgk_home=DwMFaQ=aTOVZmpUfPKZuaG9NO7J7Mh6imZbfhL47t9CpZ-pCOw=BX8us55AyPAIC_WBilHRkA=Ct0KZCwEwpWRcA5CUercOpxFrSByRm-qocG1lq-PEZc=joWXazAAemA3JtxXYrqXryS48Uko6JW70pfW7PzQSWc=>
>>>
>>>
>>>
>>> *From:* rietveld_l-requ...@ill.fr  *On
>>> Behalf Of *miguel gregorkiewitz
>>> *Sent:* Monday, January 30, 2023 7:07 AM
>>> *To:* francois Goutenoire 
>>> *Cc:* Rietveld List (rietveld_l@ill.fr) 
>>> *Subject:* Re: Sealing capillary in a glove box
>>>
>>>
>>>
>>> I constructed an electrical heater which is used with a tunable power
>>> supply and a microscope if possible. Let me know if you like to have
>>> details of the design!
>>>
>>>
>>>
>>> Miguel
>>>
>>>
>>>
>>>
>>>
>>> El lun, 30 ene. 2023 12:01, francois Goutenoire <
>>> francois.gouteno...@univ-lemans.fr> escribió:
>>>
>>> Dear Rietveld users,
>>>
>>> We are currently working with some very hygroscopic compounds in
>>> capillaries.
>>>
>>> These capillaries are fill in a glove box (N2).
>>>
>>> How can we sealed these capillaries (borosilicate) in the glove box ?
>>>
>>> Best wishes, François
>>>
>>> --
>>>
>>> *
>>>
>>> Pr. Francois GOUTENOIRE
>>>
>>> e-mail: francois.gouteno...@univ-lemans.fr
>>>
>>> Tel: 02.43.83.33.54
>>>
>>> FAX: 02.43.83.35.06
>>>
>>> Institut des Molécules et des Matériaux du Mans
>>>
>>> IMMM - UMR CNRS 6283
>>>
>>> Elaboration et Caracterisation des Composés Cristalisés (E3C)
>>>
>>> Université du Maine - Avenue Olivier Messiaen
>>>
>>> F-72085 Le Mans Cedex 9
>>>
>>> FRANCE
>>>
>>> *
>>>
>>> Formation Rietveld CNRS
>>>
>>> https://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135
>>>  
>>> <https://urldefense.com/v3/__https:/cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135__;!!P4SdNyxKAPE!E5N0CEpdBtylgCU8kLrz7ZUxzY9xMM0IJx3x3deJvBdK8Eb5EJDRl94_NUfi3eBii_ijx-PVnve4866ckg$>
>>>
>>> Formation EDX CNRS
>>>
>>> https://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135 
>>> <https://urldefense.com/v3/__https:/c

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz 
Dear Peter,

A couple of minutes ago I sent you a zip file containg the documents of our
manipulator to seal capillaries etc.

Let me know if you have any.problems!

Best

Miguel

El lun, 30 ene. 2023 19:19, Khalifah, Peter  escribió:

> Hello Miguel,
>
>
>
> I’d love to learn more about your design if you don’t mind sharing.  We
> have been thinking for a while about doing something like this.
>
>
>
> Best wishes,
>
>
>
> Peter
>
> Professor  Chemist
> Dept. of Chemistry Dept. of Chemistry
> Stony Brook University Brookhaven National Laboratory
> Stony Brook, NY 11794-3400 Upton, NY 11973-5000
>
> Office: 447 Grad. ChemistryOffice: Bldg 555, Rm 340
> Phone: (631)632-7796   Phone: (631)344-7689
> Fax: (631)632-7960 Fax: (631)344-5815
>
> Web page: https://sites.google.com/a/stonybrook.edu/pgk/home
> <https://urldefense.proofpoint.com/v2/url?u=https-3A__sites.google.com_a_stonybrook.edu_pgk_home=DwMFaQ=aTOVZmpUfPKZuaG9NO7J7Mh6imZbfhL47t9CpZ-pCOw=BX8us55AyPAIC_WBilHRkA=Ct0KZCwEwpWRcA5CUercOpxFrSByRm-qocG1lq-PEZc=joWXazAAemA3JtxXYrqXryS48Uko6JW70pfW7PzQSWc=>
>
>
>
> *From:* rietveld_l-requ...@ill.fr  *On Behalf
> Of *miguel gregorkiewitz
> *Sent:* Monday, January 30, 2023 7:07 AM
> *To:* francois Goutenoire 
> *Cc:* Rietveld List (rietveld_l@ill.fr) 
> *Subject:* Re: Sealing capillary in a glove box
>
>
>
> I constructed an electrical heater which is used with a tunable power
> supply and a microscope if possible. Let me know if you like to have
> details of the design!
>
>
>
> Miguel
>
>
>
>
>
> El lun, 30 ene. 2023 12:01, francois Goutenoire <
> francois.gouteno...@univ-lemans.fr> escribió:
>
> Dear Rietveld users,
>
> We are currently working with some very hygroscopic compounds in
> capillaries.
>
> These capillaries are fill in a glove box (N2).
>
> How can we sealed these capillaries (borosilicate) in the glove box ?
>
> Best wishes, François
>
> --
>
> *
>
> Pr. Francois GOUTENOIRE
>
> e-mail: francois.gouteno...@univ-lemans.fr
>
> Tel: 02.43.83.33.54
>
> FAX: 02.43.83.35.06
>
> Institut des Molécules et des Matériaux du Mans
>
> IMMM - UMR CNRS 6283
>
> Elaboration et Caracterisation des Composés Cristalisés (E3C)
>
> Université du Maine - Avenue Olivier Messiaen
>
> F-72085 Le Mans Cedex 9
>
> FRANCE
>
> *
>
> Formation Rietveld CNRS
>
> https://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135
>  
> <https://urldefense.com/v3/__https:/cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135__;!!P4SdNyxKAPE!E5N0CEpdBtylgCU8kLrz7ZUxzY9xMM0IJx3x3deJvBdK8Eb5EJDRl94_NUfi3eBii_ijx-PVnve4866ckg$>
>
> Formation EDX CNRS
>
> https://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135 
> <https://urldefense.com/v3/__https:/cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135__;!!P4SdNyxKAPE!E5N0CEpdBtylgCU8kLrz7ZUxzY9xMM0IJx3x3deJvBdK8Eb5EJDRl94_NUfi3eBii_ijx-PVnvce1VM6KQ$>
>
> Formation SAXS et Réflectivités pour couches minces et matériaux 
> nanostructurés.
>
> https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135
>  
> <https://urldefense.com/v3/__https:/cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135__;!!P4SdNyxKAPE!E5N0CEpdBtylgCU8kLrz7ZUxzY9xMM0IJx3x3deJvBdK8Eb5EJDRl94_NUfi3eBii_ijx-PVnvcF7Odriw$>
>
> Bibliographie
>
> https://scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=title
>  
> <https://urldefense.com/v3/__https:/scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=title__;!!P4SdNyxKAPE!E5N0CEpdBtylgCU8kLrz7ZUxzY9xMM0IJx3x3deJvBdK8Eb5EJDRl94_NUfi3eBii_ijx-PVnveBg_dzvw$>
>
> https://orcid.org/-0001-5339-3002 
> <https://urldefense.com/v3/__https:/orcid.org/-0001-5339-3002__;!!P4SdNyxKAPE!E5N0CEpdBtylgCU8kLrz7ZUxzY9xMM0IJx3x3deJvBdK8Eb5EJDRl94_NUfi3eBii_ijx-PVnvcxWOu4GQ$>
>
> ++
> Please do NOT attach files to the whole list  >
> Send commands to  eg: HELP as the subject with no body
> text
> The Rietveld_L list archive is on
> http://www.mail-archive.com/rietveld_l@ill.fr/
> <https://urldefense.com/v3/__http:/www.mail-archive.com/rietveld_l@ill.fr/__;!!P4SdNyxKAPE!E5N0CEpdBtylgCU8kLrz7ZUxzY9xMM0IJx3x3deJvBdK8Eb5EJDRl94_NUfi3eBii_ijx-PVnvcvu4nv9A$>
> ++
>
>
++
Please do NOT attach files to the whole list 
Send commands to  eg: HELP as the subject with no body text
The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/
++

Re: Sealing capillary in a glove box

2023-01-31 Thread miguel gregorkiewitz 
Dear Cristóbal,

A couple of minutes ago I sent you a zip file containg the documents of our
manipulator to seal capillaries etc.

Let me know if you have any.problems!

Best

Miguel


El lun, 30 ene. 2023 14:08, Cristóbal Verdugo 
escribió:

> Dear Miguel,
> could you, please, share details about the designt of the electrical
> heater?
>
> Thanks
>
> Regards,
>
> Cristóbal
>
>
> —
> Cristóbal Verdugo
>
> cverdu...@gmail.com
>
> Sobre 30/01/2023 13:09:48, miguel gregorkiewitz 
> escribió:
> ++ Please do
> NOT attach files to the whole list Send commands to eg: HELP as the
> subject with no body text The Rietveld_L list archive is on
> http://www.mail-archive.com/rietveld_l@ill.fr/
> ++
> I constructed an electrical heater which is used with a tunable power
> supply and a microscope if possible. Let me know if you like to have
> details of the design!
>
> Miguel
>
>
> El lun, 30 ene. 2023 12:01, francois Goutenoire <
> francois.gouteno...@univ-lemans.fr> escribió:
>
>> Dear Rietveld users,
>>
>> We are currently working with some very hygroscopic compounds in
>> capillaries.
>>
>> These capillaries are fill in a glove box (N2).
>>
>> How can we sealed these capillaries (borosilicate) in the glove box ?
>>
>> Best wishes, François
>>
>> --
>> *
>> Pr. Francois GOUTENOIRE
>> e-mail: francois.gouteno...@univ-lemans.fr
>> Tel: 02.43.83.33.54
>> FAX: 02.43.83.35.06
>> Institut des Molécules et des Matériaux du Mans
>> IMMM - UMR CNRS 6283
>> Elaboration et Caracterisation des Composés Cristalisés (E3C)
>> Université du Maine - Avenue Olivier Messiaen
>> F-72085 Le Mans Cedex 9
>> FRANCE
>> *
>> Formation Rietveld 
>> CNRShttps://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135
>> Formation EDX CNRShttps://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135
>> Formation SAXS et Réflectivités pour couches minces et matériaux 
>> nanostructurés.https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135
>> Bibliographiehttps://scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=titlehttps://orcid.org/-0001-5339-3002
>>
>> ++
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>> text
>> The Rietveld_L list archive is on
>> http://www.mail-archive.com/rietveld_l@ill.fr/
>> ++
>>
>>
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Re: Sealing capillary in a glove box

2023-01-31 Thread Francois Fauth 

Hi

Most of MSPD at ALBA users facing this problem (typically battery 
materials previously filled and sealed in Ar GB) prefer sealing with 
plastiline (instead of grease)
The problem is often sharp cutting the capillary after having filled the 
capillary  Borosilicate caps appaers more brittle than quartz.

At the end is a question of practicing.

Note that for long time in air (transport for example) it is still 
advised keeping the capillary stored in sealed envelope/containers


PS Funny coincidence, today users are collecting data on such sealed 
capillarys


Francois


On 30/01/2023 11:58, francois Goutenoire wrote:


Dear Rietveld users,

We are currently working with some very hygroscopic compounds in 
capillaries.


These capillaries are fill in a glove box (N2).

How can we sealed these capillaries (borosilicate) in the glove box ?

Best wishes, François

--
*
Pr. Francois GOUTENOIRE
e-mail:francois.gouteno...@univ-lemans.fr
Tel: 02.43.83.33.54
FAX: 02.43.83.35.06
Institut des Molécules et des Matériaux du Mans
IMMM - UMR CNRS 6283
Elaboration et Caracterisation des Composés Cristalisés (E3C)
Université du Maine - Avenue Olivier Messiaen
F-72085 Le Mans Cedex 9
FRANCE
*
Formation Rietveld CNRS
https://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135
Formation EDX CNRS
https://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135
Formation SAXS et Réflectivités pour couches minces et matériaux nanostructurés.
https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135
Bibliographie
https://scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=title
https://orcid.org/-0001-5339-3002

++
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--
Dr. FAUTH Francois Experiments Division
CELLS - ALBAhttp://www.cells.es
Carrer del la Llum 2-26
08290 Cerdanyola del Vallès, Barcelona (Spain)
Phone/Fax +34 93 592 4325 / +34 93 592 4301


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Re: Sealing capillary in a glove box

2023-01-30 Thread miguel gregorkiewitz 
I constructed an electrical heater which is used with a tunable power
supply and a microscope if possible. Let me know if you like to have
details of the design!

Miguel


El lun, 30 ene. 2023 12:01, francois Goutenoire <
francois.gouteno...@univ-lemans.fr> escribió:

> Dear Rietveld users,
>
> We are currently working with some very hygroscopic compounds in
> capillaries.
>
> These capillaries are fill in a glove box (N2).
>
> How can we sealed these capillaries (borosilicate) in the glove box ?
>
> Best wishes, François
>
> --
> *
> Pr. Francois GOUTENOIRE
> e-mail: francois.gouteno...@univ-lemans.fr
> Tel: 02.43.83.33.54
> FAX: 02.43.83.35.06
> Institut des Molécules et des Matériaux du Mans
> IMMM - UMR CNRS 6283
> Elaboration et Caracterisation des Composés Cristalisés (E3C)
> Université du Maine - Avenue Olivier Messiaen
> F-72085 Le Mans Cedex 9
> FRANCE
> *
> Formation Rietveld 
> CNRShttps://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135
> Formation EDX CNRShttps://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135
> Formation SAXS et Réflectivités pour couches minces et matériaux 
> nanostructurés.https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135
> Bibliographiehttps://scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=titlehttps://orcid.org/-0001-5339-3002
>
> ++
> Please do NOT attach files to the whole list  >
> Send commands to  eg: HELP as the subject with no body
> text
> The Rietveld_L list archive is on
> http://www.mail-archive.com/rietveld_l@ill.fr/
> ++
>
>
++
Please do NOT attach files to the whole list 
Send commands to  eg: HELP as the subject with no body text
The Rietveld_L list archive is on http://www.mail-archive.com/rietveld_l@ill.fr/
++

Re: Sealing capillary in a glove box

2023-01-30 Thread Fernando Igoa 
Dear François,

The easy way we have found to do that is by isolating the open aperture
with vacuum grease inside the glove box and theb taking them outside where
you can seal them easily with a lighter.

Hope it helps

Best,

Le lun. 30 janv. 2023 à 12:01, francois Goutenoire <
francois.gouteno...@univ-lemans.fr> a écrit :

> Dear Rietveld users,
>
> We are currently working with some very hygroscopic compounds in
> capillaries.
>
> These capillaries are fill in a glove box (N2).
>
> How can we sealed these capillaries (borosilicate) in the glove box ?
>
> Best wishes, François
>
> --
> *
> Pr. Francois GOUTENOIRE
> e-mail: francois.gouteno...@univ-lemans.fr
> Tel: 02.43.83.33.54
> FAX: 02.43.83.35.06
> Institut des Molécules et des Matériaux du Mans
> IMMM - UMR CNRS 6283
> Elaboration et Caracterisation des Composés Cristalisés (E3C)
> Université du Maine - Avenue Olivier Messiaen
> F-72085 Le Mans Cedex 9
> FRANCE
> *
> Formation Rietveld 
> CNRShttps://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135
> Formation EDX CNRShttps://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135
> Formation SAXS et Réflectivités pour couches minces et matériaux 
> nanostructurés.https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135
> Bibliographiehttps://scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=titlehttps://orcid.org/-0001-5339-3002
>
> ++
> Please do NOT attach files to the whole list  >
> Send commands to  eg: HELP as the subject with no body
> text
> The Rietveld_L list archive is on
> http://www.mail-archive.com/rietveld_l@ill.fr/
> ++
>
>
++
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Send commands to  eg: HELP as the subject with no body text
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++

RE: Sealing capillary in a glove box

2023-01-30 Thread Radovan Cerny 
Dear François,

You can just put a bit of vacuum grease, but this is not mechanically very 
stable. The best is to seal with a drop of fast epoxy glue. Easy to manipulate 
inside the glove box.

Best regards

Radovan

Radovan Cerny
Laboratoire de Cristallographie, DQMP
Université de Genève
24, quai Ernest-Ansermet
CH-1211 Geneva 4, Switzerland
Phone  : [+[41] 22] 37 964 50, FAX : [+[41] 22] 37 961 08
mailto : radovan.ce...@unige.ch
URL: 
http://www.unige.ch/sciences/crystal/cerny/rcerny.htm

De : rietveld_l-requ...@ill.fr  De la part de 
francois Goutenoire
Envoyé : lundi, 30 janvier 2023 11:59
À : Rietveld List (rietveld_l@ill.fr) 
Objet : Sealing capillary in a glove box


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Dear Rietveld users,

We are currently working with some very hygroscopic compounds in capillaries.

These capillaries are fill in a glove box (N2).

How can we sealed these capillaries (borosilicate) in the glove box ?

Best wishes, François

--

*

Pr. Francois GOUTENOIRE

e-mail: 
francois.gouteno...@univ-lemans.fr

Tel: 02.43.83.33.54

FAX: 02.43.83.35.06

Institut des Molécules et des Matériaux du Mans

IMMM - UMR CNRS 6283

Elaboration et Caracterisation des Composés Cristalisés (E3C)

Université du Maine - Avenue Olivier Messiaen

F-72085 Le Mans Cedex 9

FRANCE

*

Formation Rietveld CNRS

https://cnrsformation.cnrs.fr/diffraction-des-rayons-x-sur-materiaux-polycristallins?axe=135

Formation EDX CNRS

https://cnrsformation.cnrs.fr/fluorescence-x-edx?axe=135

Formation SAXS et Réflectivités pour couches minces et matériaux nanostructurés.

https://cnrsformation.cnrs.fr/caracterisation-des-materiaux-nanostructures-par-diffusion-des-rayons-x?axe=135

Bibliographie

https://scholar.google.fr/citations?hl=fr=qC-lmN4J_op=list_works=1=title

https://orcid.org/-0001-5339-3002
++
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Send commands to  eg: HELP as the subject with no body text
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