Re: [biofuel] Re: Reclaiming the methanol

2001-05-31 Thread Paul Gobert
- Original Message - From: Gary and Jos Kimlin [EMAIL PROTECTED] Subject: Re: [biofuel] Re: Reclaiming the methanol Paul my next batch will be with cotton seed oil. I intend to use the twostage with KOH rather than NaOH. The best I can do with NaOH seems to be 80-85% pure, Pure

Re: [biofuel] Re: Reclaiming the methanol

2001-05-31 Thread Keith Addison
Any experience using glycerin as a heating fuel? Afraid not but very interested in same. With winter begining and an aging slow combustion stove I,m looking for alternatives. Some interesting postings on this subject over last month or so. Regards , Paul Be sure you have efficient combustion

RE: [biofuel] Re: Reclaiming the methanol

2001-05-29 Thread kirk
$2 a pound for KOH? How much does KCl cost? -Original Message- From: Gary and Jos Kimlin [mailto:[EMAIL PROTECTED] Sent: Monday, May 28, 2001 5:26 AM To: biofuel@yahoogroups.com Subject: Re: [biofuel] Re: Reclaiming the methanol Paul my next batch will be with cotton seed oil. I intend

RE: [biofuel] Re: Reclaiming the methanol

2001-05-29 Thread jerry dycus
Hi All, For those who are reclaiming methanol what % of the methanol do you get back? I assume vacuum recovery method. Thanks, jerry dycus __ Do You Yahoo!? Yahoo! Auctions - buy the things you

Re: [biofuel] Re: Reclaiming the methanol

2001-05-28 Thread zh24mij
Paul, one vessel would be great, but poses (at first glance) two problems: Time and batch quantity, which is to say that you'd be producing a smaller batch over a longer period of time. Sure, it's compact, but for a garage operation I'd prefer a multi-barrel approach

Re: [biofuel] Re: Reclaiming the methanol

2001-05-28 Thread Gary and Jos Kimlin
Paul my next batch will be with cotton seed oil. I intend to use the twostage with KOH rather than NaOH. The best I can do with NaOH seems to be 80-85% pure, I suspect that leaves too much water to avoid soaps. I'll take your advice and wash and dry it. I'll let you know how it goes. The oil

Re: [biofuel] Re: Reclaiming the methanol

2001-05-27 Thread Paul Gobert
- Original Message - Treat anything clear as Methanol. My first attempt making biod, just sucking in Meth and at a temp of 55oC I found at least 250ml of Meth in my liquid trap. Be very careful. Ian Ian, In my trial laboratory scale batches have found that methoxide and SVO

[biofuel] Re: Reclaiming the methanol

2001-05-26 Thread scrof
I think you may be near the correct answer for a mixture only of water and methanol. The boiling point of mixtures can be calculated, but are easier to find experimentally. However, in recovering methanol from biodiesel byproduct we have a much more complex mixture. Any water in the mix is

[biofuel] Re: Reclaiming the methanol

2001-05-26 Thread scrof
Sorry, Mike, I didn't make it very clear, did I? I've used much more than 30 gallons in processing fuel. In total, I have recovered and reused about 30 gallons. Dale --- In [EMAIL PROTECTED], Mike Brownstone [EMAIL PROTECTED] wrote: Dale, Isn't there any loss of methanol during

[biofuel] Re: Reclaiming the methanol

2001-05-25 Thread scrof
I've used and re-used about thirty gallons of methanol so far using my hot pink vacuum still. At first I was worried about recovering water at the end of a run, so watched the condensate closely for any sign of cloudiness. I've never seen any. I don't think water can be recovered from the

[biofuel] Re: Reclaiming the methanol

2001-05-25 Thread Keith Addison
I've used and re-used about thirty gallons of methanol so far using my hot pink vacuum still. At first I was worried about recovering water at the end of a run, so watched the condensate closely for any sign of cloudiness. I've never seen any. I don't think water can be recovered from the

RE: [biofuel] Re: Reclaiming the methanol

2001-05-25 Thread Mike Brownstone
Subject: [biofuel] Re: Reclaiming the methanol I've used and re-used about thirty gallons of methanol so far using my hot pink vacuum still. At first I was worried about recovering water at the end of a run, so watched the condensate closely for any sign of cloudiness. I've never seen any. I don't

Re: [biofuel] Re: Reclaiming the methanol

2001-05-25 Thread David Teal
Dale is right, recovered methanol is OK to re-use. I have found that from biod made using 15% meth (v/v WVO), the glyc. yields 3% meth (v/v WVO) and is well worth the trouble of simple distillation at 70 deg C. Probably will use 20% in future for an easier life without unnecessary loss of