Ken,
  Sorry, but I can't make heads or tails of Frank's test results--can
you translate them into plain english? I'd like to know, not sure if
my Ole Bob thermal stir series 2 is the same version you made your
test batches with, but I am having the same large (almost half of the
PWT reading at auto shut off) drop in uS after a few days storage. I
had been kinda surprised a the large drop in conductance. But given my
idiosyncratic problems making clear CS, I just had figured it was
something unique to here.
TIA,
paula


----- Original Message ----- 
From: "Ode Coyote" <[email protected]>
> >At 03:57 PM 11/30/2003 -0500, you wrote:
> >>Ode,
> >>
> >>Here are the test results for your samples from the ICP/AES.
> >>
> >>
>  These batches [#1+#2] were run totally plug n play / absolute
neglect in a
> beaker and added together to form an average, .
>
> >>Sample        Total Silver        Ionic Silver        % Ionic
> >>Conductivity
> >>   #                    ppm                ppm
> >>(uS/cm)
> >>
> >>1-2                 11.29                 9.68                85.7
> >>12.6
>
>  This batch was totally plug n play/ absolute neglect in a pint
canning jar
> allowed to sit for 8 days in clear glass. It could have used a
stir/reset
> sequence.
>  My record:
> Off at 17 uS @92.2 deg F dropping to 8.5 uS in 8 days.
>
>  The result:
> >> 3                     9.25                 9.12
98.6
> >>8.5
> >>
> >>
> >>
> >>ICP/AES Measurements:
> >>
> >>1. Each measured value was an average of three individual
measurements. Each
> >>individual measurement was taken from three replicates of 10
seconds each.
> >>Total integration time per measured value (3 x 3 x 10 seconds) is
90
> >>seconds.
> >>
> >>2. Measured made using the silver emission spectral line at
328.068 nm
> >>
> >>3. Calibration: blank ( 0.00 ppm) and 10.00 ppm - linear from 0 -
30.00 ppm
> >>(minimum)
> >>
> >>3A. Measurement error (95% confidence) is less than: 0.05 ppm
> >>
> >>4. Particles were removed from samples by application of 365,000
G-forces
> >>for 15 minutes.
> >>
> >>
> >>Particles size distribution plots will be done in the next few
days and the
> >>.pdf files will be emailed to you.
> >>
> >>
> >>Francis Key, Principal Scientist
> >>Colloidal Science Lab. Inc.
> >>Westampton, NJ 08060
> >>609.267.2065




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