----- Original Message ----- 
From: "Matthew McCann" <[email protected]>
To: "William Amos" <[email protected]>
Sent: Saturday, November 27, 2004 3:29 PM
Subject: Re: Re:CS>Silver lining and silver production


> Hello, William,
> 
> I do not use a commercially-made electrolysis
> apparatus. At one time I used current regulation,
> but I went to current limitation at a low current
> range (20-200 microamperes) instead. I get a
> low current by keeping my electrodes separated
> more than most people do (about 3 inches.)
> I do current limitation by putting a rheostat in
> series with my reaction vessel electrodes, power
> supply (a 30vdc external power supply salvaged
> from a discarded Apple computer) and analog
> microammeter (range: 0 to 500 microamperes.
> The resistance of the rheostat (a variable resistor)
> can be about the same as the resistance between
> electrodes in DW before 'starter' is added. I then
> adjust the rheostat so that it the current goes to
> about 50% to 60% of full-scale reading on my
> analog microammeter when the brew is done.
> As it turns out, a 100 kilohm or 200 kilohm
> rheostat works well with the rest of my apparatus.
> I like to keep the current limitation below 500
> microamperes so I can let it brew all night as well
> as reduce particulate size range. I consider current
> range to be more important than current constancy.
> 
> It takes more time to prepare a batch of EIS this
> way. But a always keep a gallon or two on hand.
> If I don't use it up in several months, I don't discard
> it. I just rebrew it. I can tell when it is done by the
> appearance of a shiny slick on top of the brew.
> This is a natural end-point indicator. This slick is
> highly reflective but probably only one molecule thick.
> Much of it can be re-dispersed by stirring with a
> glass rod or tube. What does not disperse can be
> concentrated at the center of the vessel by
> stirring; it can then be removed without
> filtering by sucking it out with a plastic straw or
> glass tube. After that, the brew can be left to
> stand overnight to stabilize (with electrodes removed)
> and re-brewed the next day. Re-brewing can be
> repeated quite a few times. I've done it 8 to 10 times
> until it got a yellow tinge. Then I clarify the yellowishness
> with about 1-2 cc of 3% h2o2, letting the h2o2 react
> overnight. The product is mighty strong at this point,
> but can always be diluted with DW.
> 
> Stirring is essential, and I use the thermal stirring method.
> My glass spaghetti canister sits neatly in a desktop hot-pot (West Bend,
> 600W max) at its lowest setting, on a glass
> candle holder as a spacer to reduce the heat further,
> getting a steady-state 97-101 degreese Fahrenheit.
> I conjecture that the thermal method of stirring is
> conducive to the shiny slick appearing before sediments
> do, which makes it easier to detect an end-point and
> preparing for re-brewing. But I haven't really made
> conclusive observations about this comparative
> aspect of stirring methods.
> 
> Well, I hope these comments are of interest to you.
> I think it would be good if others too would summarize
> there experiences and 'best practices.'
> 
> Best regards,
> 
> Matthew
> 
> ----- Original Message ----- 
> From: "William Amos" <[email protected]>
> To: <[email protected]>
> Sent: Saturday, November 27, 2004 2:19 PM
> Subject: Re:CS>Silver lining and silver production
> 
> 
> > Can you comment on the current limiting device ?
> > I too wondered about that.
> > Bill Amos
> > --------------------------------------------------------------
> > Hello, Max,
> >
> > I use the Canadian coins as electrodes, too. Instead of
> > reshaping them, I mount them on the lip of the reaction
> > vessel (I use a tall, narrow glass spaghetti jar) using
> > S-shaped silver wire hooks. I drilled two holes through
> > each coin, diametrically opposed and near (about 3
> > millimeters) to the edge of each coin. Two holes
> > instead of one allows me to flip the coin around
> > occasionally for an even wear. I use a brass-bristled
> > brush to clean and polish the electrodes after each use.
> > ( I use brand-new detailing brushes from an automotive
> > supplies store.) One of the advantages of coins over
> > wire is that the rigid coins hold up better to brushing.
> > There is some loss of silver from the electrodes due
> > the hole-drilling and brass-bristle brushing. But silver
> > is not expensive in comparison to the cost of distilled
> > water. I simply invested ten to eleven dollars in an
> > extra Canadian Maple Leaf. One 30-gram electrode
> > will eventually be dispersed in several thousand kilograms of distilled
> water, costing hundreds or thousands of
> > dollars depending on the source of the DW.
> >
> > Best regards,
> >
> > Matthew
> >
> 


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