Hello,

I have been using ASAPRatio from previous versions of the TPP successfully.
 However, now I cannot obtain appropriate data for the ratios with the
version present in 4.7.  ASAPRatio is not appropriately matching the
corresponding heavy labeled peptide with its light partner.  It is choosing
a peptide partner with a mass delta that doesn't make sense.

I am labeling amines by reductive alkylation with acetone (D0 and D6).  I
use Tandem for the search and specify the mods as per the API instructions
where I specify static mod of 42@[ and 42@K and potential mods of 6@[ and
6@K.

In ASAPRatio setup, I specify the following (via Petunia not the command
line):

xinteract -Ninteract.pep.xml -p0 -l5 -Op -dDECOY
-A-lnK-b-r0.5-mn48.0846K176.1795

Depending on the charge the mass delta between the light and heavy will be
multiples of 6 for each labeled site, but I'm seeing multiples of 48
instead and so the h/l pairs are not correct.

I am not certain if this is a problem with ASAPRatio, is it a newer version
than what was in 4.6, or if it has something to do with the output of
Tandem.  If the former I can go and replace the new version of ASAPRatio
with an older version and see if that fixes it.

Any help much appreciated.

Brian



Brian Hampton
Protein Analysis Lab
Center for Vascular and Inflammatory Diseases
University of Maryland School of Medicine
655 West Baltimore Street BRB 7-018
Baltimore  MD  21201
V: 410-706-8207

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