Dear Joshua

It is good to see your project "coming together!"

I have deleted stuff that does not include a specifgic comment from me... see below...

Quoting Joshua Guinto <[email protected]>:

Dear Crispin and Kevin

...del...

To respond to some of Kevins question.

they are in between the lines...

2012/9/19 Kevin C <[email protected]>


Dear Jed

...del...

I might be able to help with operation of the distilling aspects of your
project.

1: Is it a continuous process or a batch process?
It is a batch process, one load is about 115 liters .



3: What percentage of ethanol do you want in your final distillate product?

Hmmm right now, the latest test indicates 70 percent with the traditional
methods We want to increase that to as much as 90 %.

# With a reflux column, you can get between 90% to 95% without difficulty. A big advantage of trying for 95% is that it basically eliminates contaminants, such as fusel oils, butanol, propanol, and methanol.

4: Do you use a simple condenser, where you simply condense all the vapor
that is boiled off, or do you use a reflux column?

We use a simple condenser. Actually, i have a clay condenser fabricated.
But i neglected to have the inside walls glazed. So i will only use that
until it is glazed. For the meantime we will use the metal condensers that
the locals fabricate themselves.

# A simple condenser does not give nearly as good a separation as does a reflux column. I would suggest that you are far better off going to a reflux column, to virtually eliminate the undesirable impurities in the distillate, and to yield a much more concentrated and pure ethanol.


5: What is the initial alcohol content of the "feed wine?"


That i wll check tommorow.

# I would guess that it is about 12%. A ferment with sufficient sugar to yield only 12% alcohol ferments out quickly, while one that has sufficient sugar to eventually permit say 15% is much more difficult to ferment to completion, and takes disproportionately longer. You can ferment to these higher alcohol contents, but you have to add appropriate yeast nutrients. Unless you have access to a Microbiologist, you are probably better off targeting for 12% alcohol maximum. You should also have a hydrometer, to measure the specific gravity of the ferment.

6: How many litres per hour of "feed wine" do you wish to process?

Sixteen liters in one hour will already be satisfying.

# This will basically depend on your firing rate. Assuming that your boiler has about 4 square meters of area, your heat input rate to the batch could be as much as about 40 kw. Very roughly, this would need about 60 kW of input energy, allowing for combustion losses and stack temperature loss. This would require a fuel burn rate of about 12 kg dry fuel equivalent per hour. You should fire it at " as much as possible", consistent with complete combustion (no smoke in the stack) and a maximum stack temperature of about 200 C. NOTE: These calculations are rough; they are generally proportional to area for a steel drum, but the pottery walls will have higher heat flow resistance, and consequently, with the same outside temperature, would have lower heat input rates to the batch. For your first "test run", you could start off with a "batch of water", and measure its rate of temperature rise, to determine the actual heat input rate to teh batch.

I don't understand your separating technology. What is condensed or cooled
in the "Radiator?"

The radiator was meant to cool off he cooling water that runs on top of the
condenser so we may use them again in a continuing cycle.

# Good move!! You don't have to haul in, or pipe in, as much cooling water.

What is the source and  nature of the "waste water" that is being sent to
the "Waste Water Treatment tanks?"

This would be the distillate, the spent liquid after the distillation. I
would not want them disposed directly to the creeks.

# You could probably re-use the "spent batch" several times as make-up for the next batch. This would reduce your treatment cost and effort.



You would probably benefit from Thermometers at various points in the
still and condensers. You should also have valves in the water cooling
pipes, to regulate the flow rate of water from your head tank.


Yes, i agree. I think i will do a monitoring chart for every point ...

# I would suggest:
1: Stack temperature... 0 to 250 C
2: "Final vapor temperature to the "final condenser." 0-100 C
3: Water temperature around reflux condenser jacket. 0-100 C
4: Temperature of vapor entering the reflux condenser. 0-100 C

# get thermometers with at least a 4" diameter dial for ease of reading. Calibrate them in a hot water bath, so that you have confidence in what each thermometer really indicates.

Am I correct in assuming that your "Radiator Assembly" cools your
condenser or reflux column water flow, to permit re-use? If so, you could
use a radiator or two (depending on how much heat you have to dissipate)
from scrapped automobiles for cooling the condenser water for re-use.


Good idea. For now im using a simple fine net like those of the mosquito
nets. I do not know if it will not melt off

# Is this basically an evaporative cooler? If so, it may not work very well if your ambient temperatures and relative humidities are high.

Your pottery boiler looks great! I presume you are using it, to minimize
differences in operation from the technology presently being employed.


The present technology is actually the use of metal drums they get from the
industries..... They could contains remains of chemicals, diesel, oil,
shampoo or anything. they clean the drums very crudely. The drums lasts
only for several months because of metal fatique. Then they wlll have to be
replaced.

The clay boiler is actually going back from the modern to the more native.

# 30 or 45 gallon drums with a clamping lid are easy to clean. However, you do need a good gasket, to avoid loss of alcohol vapor and a possible fire or explosion. Bung type drums are very cheap, and with careful washing, they should be acceptable. I am guessing that if the bottom fails, it is not so much from fatigue, but rather, from overheating as a result of organic deposits resulting from feed that was not adequately settled before feeding to the boiler. Periodic cleaning of the inside of such a boiler should extend its life.

Best wishes,

kevin

Best wishes,

Kevin Chisholm


Thank you both once again. More news  to come


Jed

Quoting [email protected]**:

 Dear All

With all respects, i wish to join in the discussion with my own concern
similar to that of Josh Kearns.

Im at present building an improved wine distillery in favor of the small
nipa wine producers in my hometown. The constructin is now in full scale
and
so im beginning to really get worried about the integrity of my design.

I do not have enough engineering background on this and do not have much
equipments. So i would really appreciate it if you could also guide me
through with this project.

I attached some photos and drawings of the project.

It was organized by a Japanese  JICA volunteer and will help more than 200
wine producers not to mention their health and the immediate environment.

Best regards

JEd Guinto

2012/9/16 Paul Anderson <[email protected]>

Josh,

From experience, having the heat go through a single pipe/chimney in the
center of the water tank is much better than having  the heat go around
the
outside of the steel drum.    And it is much less expansive.





Paul S. Anderson, PhD  aka "Dr TLUD"
Email:  [email protected]   Skype: paultlud  Phone: +1-309-452-7072
Website:  www.drtlud.com

On 9/14/2012 11:36 PM, Josh Kearns wrote:

I'm thinking about building a 5-gal TLUD fired 55-gal water heater for
outdoor showers. I'm wondering if anyone has a ballpark estimate for heat
transfer efficiency w/ and w/o using a pot skirt attachment. The hot water
tank will be a 55-gal steel drum, so I think the setup is pretty analogous
to a cookstove setup, just bigger.



20%?



Any thoughts are helpful, rough estimates OK.....thanks!





FYI, the char from the water heating setup will be used in arbor-loo style
modular composting toilets. This infrastructure is being installed during
a
rambo design-and-build sesh for my wedding on a farm in rural Appalachia
(USA), but will be used continually by future events at the site. Cool,
huh?!?!



Josh




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