I have just completed another test batch with the re-titrated oil and got a thin layer of by-product glycerine at the bottom of the Masson jar. Of course this may be attributed to the supplement of WVO I tossed into the frey or it is residual from the first process or a combination of both. Had I been a little more foresoughtful I would have simply re-processed the original lot as Todd suggested once to see if any glyc remained, but "I" wanted to have a round number (!) so now I will let that settle until tomorow and continue with the quality shake test. That should do it. In the kitchen I can control the heat and mixing easily, so now I have to translate that to the larger volumes. Friday will tell if I got it right or not when I re-process the entire 2o liter batch using the new titration numbers. The NaOH is disolving in the methanol as we speak and should be ready for when I am ready to use it.
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