Hi Attila,

I got to thinking some more about the DUT, and what's inside, and the parasitics. I found ref [2] that you showed in the OP, about the HP resistance standards. It's very informative, covering a lot of the construction details. One thing that struck me is the discussion of transient performance beginning on page 12, noting that chemical contamination in older (non-HP) types is known to cause an electro-chemical cell effect that can last for many seconds. I think you said your resistor is an old type, similar to the HP ones. I wonder if maybe this is the cause of trouble.

To eliminate all possible DUT problems, I'd suggest setting it up with just a regular, medium precision 10 K resistor, like a T9 with wire leads. For quick, temporary use, you can scrape off the lead plating down to bare copper, then tightly twist the lead and copper wires to the 3458A, then crimp a splice lug on to crush them together for a gas-tight seal. Even a (steel-insert) wire nut will do to hold it together for a while, as long as there's good Cu-Cu contact between all the parts. Then you can suspend the little DUT up away from everything, and mostly eliminate the parasitics, packaging, and other issues. If it works with this, but not the original DUT, you'll know what the deal is.

Ed
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