[biofuel] Have I made biodiesel?

2004-07-09 Thread Thomas Kelly

Have I succeeded in making biodiesel?
 I Last Fall I attended a workshop on producing biodiesel and was given a 
recipe.A few days ago I decided to give it a try. 
 I used a gallon (3.78L) of corn oil from the market. Unable to find any 
NaOH, I used KOH instead. I used plastic milk containers for mixing, reacting, 
and washing. It was crude I admit, but the results are:
 - 600ml  clear, reddish-brown liquid on bottom
 - about 3L of cloudy, golden liquid on top
 I poked a hole in the bottom of the milk container and drained out the 
glycerine
 After several washings the golden liquid on top is now a beautiful clear 
liquid.Biodiesel?
 My questions:
  The reddish-brown liquid never solidified, even after refrigeration. Is 
it glycerine?
  The pH of the wash water finally reached  7. However the water is still 
coming out cloudy, Will the wash water ever come out clear?
   Should I test the product in my brother-in-law's BMW?

 Thanks,
Tom
  

   

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Re: [biofuel] Have I made biodiesel?

2004-07-09 Thread Keith Addison

Hello Tom

Have I succeeded in making biodiesel?

Yes. It's a good start, well done, congratulations.

However, there are a lot of things you don't say and that might need 
attention when you take your next step. How much KOH (or NaOH) and 
how you measured it, how much methanol, how you mixed the methoxide, 
the processing temperature you used, how and how much you agitated 
it, for how long.

 I Last Fall I attended a workshop on producing biodiesel and 
was given a recipe.A few days ago I decided to give it a try.
 I used a gallon (3.78L) of corn oil from the market. Unable to 
find any NaOH, I used KOH instead. I used plastic milk containers 
for mixing, reacting, and washing. It was crude I admit,

To continue on an upward path rather than a downward one, please read 
this and then just keep going from there:

Start here:
Where do I start?
http://journeytoforever.org/biodiesel_make.html#start

but the results are:
 - 600ml  clear, reddish-brown liquid on bottom
 - about 3L of cloudy, golden liquid on top
 I poked a hole in the bottom of the milk container and drained 
out the glycerine
 After several washings the golden liquid on top is now a 
beautiful clear liquid.Biodiesel?
 My questions:
  The reddish-brown liquid never solidified, even after 
refrigeration. Is it glycerine?

Partly. It's a mixture of crude glycerine, soaps (from neutralised 
Free Fatty Acids), excess methanol, and the catalyst (KOH).

This by-product cocktail is very unlikely to solidify if you use 
KOH as a catalyst (one of the advantages of using KOH). If you had 
the idea that it has to solidify, whichever catalyst you use, you 
were wrongly informed. Please see:

How much glycerine? Why isn't it solid
http://journeytoforever.org/biodiesel_make2.html#howmuchglyc

I strongly suggest you read everything on the two Make your own 
biodiesel pages as well as all the further information linked from 
them.

  The pH of the wash water finally reached  7. However the water 
is still coming out cloudy, Will the wash water ever come out clear?

Keep going until it does, and take it as further indication that it 
was crude, as you say, and needs improvement.

   Should I test the product in my brother-in-law's BMW?

When you've finished washing it and settling it, yes. Even if he's 
bigger than you, LOL!

Best wishes

Keith


 Thanks,
Tom




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