Hello.
You are doing the right thing. But, remember that a high FFA content
usually is managed with NaOH or KOH in excess or by a pre-staged acid
transesterification. Water is not.
Best regards
Jan Warnqvist
AGERATEC AB

[EMAIL PROTECTED]

+ 46 554 201 89
+46 70 499 38 45
----- Original Message ----- 
From: <[EMAIL PROTECTED]>
To: <[EMAIL PROTECTED]>
Sent: Sunday, March 06, 2005 4:20 PM
Subject: Re: [Biofuel] A problem with WVO


> Quoting Jan Warnqvist <[EMAIL PROTECTED]>:
>
> > Hello.
> > I think that both the FFA content and water content are too high in that
> > oil. The water content is the worst enemy for a good
trans-etherification.
> > Try this :
> > Put the oil in a vessel at 70oC for 24 hrs. The water may form a
separate
> > phase at the bottom of the vessel.
> > Check the water content. ExxonMobile sells a nice kit called Mobil water
> > test. The active chemical compound in this is calciumdihydride. It is a
> > reliable method. Do not try to transesterify again until the water
content
> > is around 0,5%.
> > And- watch out for any remaining detergents in the oil !
> > Jan Warnqvist
> > AGERATEC AB
> >
> > [EMAIL PROTECTED]
>
> Hi Jan,
>
> I think my main problem is too much free fat in the oil. If I add 20-25%
of it
> to my other soy oil that is little used for only two days at a street
fair,
> then it converts really well, as the overall free fat content of the
blended
> batch is low enough to work with just a one step lye/meth conversion. SO,
I am
> going to move to a two step acid/meth-lye program with it. Watr saeems not
to
> be a big issur here in the desert, but since you guys warned me, I'll sure
> check for it!!
>
> Thanks again SO MUCH and let's keep working to save our country from those
> that run it!!
>
> kitch in Az.
>
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