Richard Gillilan wrote:



I am currently working on guidelines for when helium and microbeam are necessary (based on both simulations and explicit measurements). At the present time, my feeling is that crystals below 50 micron can certainly make the extra hassle worthwhile. It really depends upon how badly you want that extra resolution. In the case above, it pushed the resolution from above to below the 2.0 Angstrom mark based on I/SIG.

Hi Richard,

I/SigI based on which program ? Default modes or tweaked by expert ? I would give this particular dataset a chance to be processed by all available programs and then do the comparison, or actualy all the datasets you have with various setups. Should be a nice table comparing program X versus Y and Z with the given data. And if it's SeMet data that would even be better - runnig e.g. Shelx and demonstrating which setup leads to an interpretable electron density.

Juergen

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Jürgen Bosch
University of Washington
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