Hi everyone,
I have recently been plagued by incomplete data according to HKL2000. My last
dataset, which is 360 degrees of images, with < 0.1% rejected during scaling,
and no overlaps during indexing/integration, keeps on scaling in HKL2000 as
incomplete. It is reported incomplete only at higher resolution (see stats
below, in my case 5 Angstroems is usually high resolution). This is really odd,
because (1) the data is 360 degrees, (2) if the beamstop was the culprit, I
would expect incompleteness at low res., not high, and not 35% incomplete, (3)
at this resolution the blind region outside the Ewald sphere should be
insignificant (not 35%), (4) and there are no overlaps (thanks to the detector
being sent to "Outer Mongolia", according to our synchrotron host), and (5)
there are no overloads. Moreover, mosflm thinks the data is 100.0% complete. I
have had similar incompleteness issues on other unrelated low resolution data
in the last year or two with HKL2000.
So before I lose it because of HKL2000, I have two questions, and I'd
appreciate any answers to either:
1. Can there be another reason for incompleteness that I am missing (other than
blind region at higher res., overlaps, overloads, and "not enough many frames")?
2. Has anyone been experiencing similar phenomena with HKL2000 (v0.98.698o)?
Especially with anisotropic data?
Thanks,
Engin
Shell Summary of observation redundancies:
Lower Upper % of reflections with given No. of observations
limit limit 0 1 2 3 4 5-6 7-8 9-12 13-19 >19 total
50.00 11.49 0.1 0.1 3.7 2.9 93.3 0.0 0.0 0.0 0.0 0.0 99.9
11.49 9.14 0.0 0.0 1.7 2.3 96.0 0.0 0.0 0.0 0.0 0.0 100.0
9.14 7.99 0.0 0.0 1.5 2.8 95.7 0.0 0.0 0.0 0.0 0.0 100.0
7.99 7.26 0.0 0.0 1.5 2.8 95.7 0.0 0.0 0.0 0.0 0.0 100.0
7.26 6.74 0.0 0.0 1.3 2.2 96.6 0.0 0.0 0.0 0.0 0.0 100.0
6.74 6.35 0.0 0.3 1.3 4.1 94.3 0.0 0.0 0.0 0.0 0.0 100.0
6.35 6.03 2.1 3.6 4.0 7.3 83.0 0.0 0.0 0.0 0.0 0.0 97.9
6.03 5.77 8.9 6.2 5.1 10.2 69.6 0.0 0.0 0.0 0.0 0.0 91.1
5.77 5.54 16.0 6.1 6.6 9.4 61.9 0.0 0.0 0.0 0.0 0.0 84.0
5.54 5.35 20.6 7.3 6.5 6.4 59.2 0.0 0.0 0.0 0.0 0.0 79.4
5.35 5.19 25.7 6.8 6.6 7.9 52.9 0.0 0.0 0.0 0.0 0.0 74.3
5.19 5.04 26.1 5.9 6.2 7.2 54.6 0.0 0.0 0.0 0.0 0.0 73.9
5.04 4.91 28.7 7.9 6.2 7.0 50.2 0.0 0.0 0.0 0.0 0.0 71.3
4.91 4.79 29.0 7.7 5.8 7.3 50.2 0.0 0.0 0.0 0.0 0.0 71.0
4.79 4.68 32.4 7.2 7.0 7.2 46.3 0.0 0.0 0.0 0.0 0.0 67.6
4.68 4.58 31.8 9.2 7.5 6.6 44.9 0.0 0.0 0.0 0.0 0.0 68.2
4.58 4.49 35.1 9.7 6.1 6.1 43.0 0.0 0.0 0.0 0.0 0.0 64.9
4.49 4.40 33.8 11.2 7.0 6.4 41.7 0.0 0.0 0.0 0.0 0.0 66.2
4.40 4.32 37.9 9.4 7.7 7.8 37.3 0.0 0.0 0.0 0.0 0.0 62.1
4.32 4.25 36.7 11.5 8.5 6.8 36.4 0.0 0.0 0.0 0.0 0.0 63.3
All hkl 18.3 5.5 5.1 6.0 65.1 0.0 0.0 0.0 0.0 0.0 81.7
