Blow's book is excellent. 

Another good one is Practical protein crystallography by Duncan McRee 1999 
Academic 
Press. Its ever so slightly out of date on software, but the basics don't 
change. I think its an 
easier read for new crystallographers.

Also, check out some great web sites: The Cambridge University Protein 
Crystallography 
Course  http://www-structmed.cimr.cam.ac.uk/course.html

and

Berhnard Rupps web site http://www.ruppweb.org/

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