My best guess would be acetylation/propionylation with the oxygen pointing into 
the top small green density. 

cheers

Ajit B.



----- Original Message -----
From: Christian Biertuempfel <[email protected]>
Date: Tuesday, June 29, 2010 2:54 pm
Subject: [ccp4bb] density quiz
To: [email protected]


> Dear all,
> Does anyone have an idea what this density at a lysine residue could be?
>   The structure is a protein-DNA complex and I suspect that something
> left-over from the DNA synthesis reacted with the amino group even
> though the DNA substrate was purified.
> 
> christian
> 
> p.s. The protein has seen the following substances during purification
> and crystallization: Leupeptin, Pepstatin, AEBSF, MES, Tris, HEPES, DTT,
> EDTA, imidazole, glycerol, PEG 2K-MME, Mg2+, Na+, K+, Ca2+, Cl-.
> 
> 
> _______________________________________________________________________
> 
> Dr. Christian Biertümpfel
> Laboratory of Molecular Biology
> 
> NIDDK/National Institutes of Health              phone: +1 301 402 4647
> 9000 Rockville Pike, Bldg. 5, Rm. B1-03          fax:   +1 301 496 0201
> Bethesda, MD 20892-0580
> USA
> _______________________________________________________________________

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