Dear crystallographers,

I have a question concerning effective concentration. Say you have a
crystal structure whereby two loops, each part of a different domain but
within the same molecule happen to be juxtaposed and can form an
interaction.  The loops have some degree of flexibility, but are ordered
when interacting. The domains on which they are attached have a rigid
configuration due to the remainder of the structure. The interaction is
potentially very weak and mainly driven by the fact that the effective
concentration is extremely high.

The question: how can one obtain a rough estimate of the effective
concentration of these two juxtaposed loops?   The simple straightforward
answer would be to just divide number (1 each) by volume (some box drawn
around the loops), and convert this to molar. That's easy. However, this is
over-simplified and really an underestimate of 'effective' concentration,
because these loops cannot rotate freely when attached to the domains.
 Hence, there are constraints that allow them to interact more readily
compared to the isolated loops within the same box. So I'm looking for a
model that also takes limited conformational freedom into account.

If anybody has any pointers to some reference text or paper that has
performed such an analysis, I would be very interested.

Regards,

Filip

-- 
Filip Van Petegem, PhD
Associate Professor
The University of British Columbia
Dept. of Biochemistry and Molecular Biology
2350 Health Sciences Mall - Rm 2.356
Vancouver, V6T 1Z3

phone: +1 604 827 4267
email: [email protected]
http://crg.ubc.ca/VanPetegem/

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