OK they looked similar in your pictures

Maybe you have two different crystal forms

Phil

On 30 Dec 2014, at 16:56, "<Thii Chand>" <[email protected]> wrote:

> Dear Dr.Evans, 
> 
> Thanks for your reply.
> 
> The unit cell parameters are a=140 , b=110, c=44., Hence i am afraid, the 
> interchange couldn't have occurred due to similar a and b. I had performed 
> dehydration using PEG in the said case. I agree that dehydration or soaking 
> with ligand can hardly lead to the interchange of axis.But, what i find 
> difficult to understand is how come only in three out of nice 
> structures,interchange of cell axis occurs, where i had maintained similar 
> experimental conditions for all the nine cases.  Is there any logical 
> explanation for this or am i doing something wrong?
> 
> The sp group are P21212 in all the cases.
> 
> Thanks in advance 
> 
> Regards, 
> T.chandran

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