The precision or significance of rfree depends on the number of reflections
used to calculate it. No fixed rule for percentage exists. Tickle & Brunger
have elaborated on this. References pp 625 in bmc. Depending on how many
data overall you have and can set aside, for an overall rfree uncertainty
of approx 1% several 100 to 1000 suffice. If you just use rfree as a
qualitative tool, criteria are less stringent  than using it for
quantitative estimates.

Best br











On Tue, Jul 10, 2018, 10:06 张士军 <[email protected]> wrote:

> Dear all
>
> I am confusing the choose of free
> R-flags recently. Rfactor means calculatted from reflection not used in 
> refinement,so what's big the
> difference between different percentage of R-flags,like it's about 5% in ccp4
> -refmac, while it is
> 10% in phenix-refinement,what's the difference between them and how they 
> affect the
> Rwork and Rfree values when do refinement. Thanks a lot !
>
> best regards
>
> shijun
>
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