Thank you Robbie! A bit clearer now to me..

On 10 September 2018 at 11:19, Robbie Joosten <[email protected]>
wrote:

> Hi Eleanor,
>
> You point out two major problems with PDB files. The TER record nightmare
> is pretty bad. Although it seems that at least now they are written by
> programs, they end op at the weirdest places due to aggressive addition of
> the TERs. At the same time, they are sometimes missing when there are for
> instance (mono/di)peptide ligands. The problem is that most programs that
> write PDB files are not aware of the sequence of entire protein. That, or
> they just blatantly ignore it. This should work better in mmCIF as long as
> programs enforce the presence of a sequence for the macromolecular
> entities.
>
> The charges thing has been getting on my nerves lately because most of the
> time it is a load of dingo's kidneys. There is no localized integral charge
> on the NH atoms of ARG! Neither is there for ASP and GLU sidechains,
> especially not a 1+. The PDB is aware of the problem now, but the source of
> these charges is not obvious. They do not seem to come from refinement
> programs, but these programs do use the charges to modify the scattering
> factors and write them out again. One hopes that this problem is solved
> soon.
>
> Sorry for straying off topic.
>
> Cheers,
> Robbie
>
> > -----Original Message-----
> > From: CCP4 bulletin board <[email protected]> On Behalf Of Eleanor
> > Dodson
> > Sent: Monday, September 10, 2018 12:03
> > To: [email protected]
> > Subject: Re: [ccp4bb] unexpected errors in LSQKAB
> >
> > Eugenere - are you responsible for mmdb?  Could these features cause
> > problems?
> > Eleanor
> >
> >
> > The PDB file Thern_tRNA has some anomalies -
> >
> > 1) several unneeded TER cards
> >
> > TER     399      LYS A  52   - there is a chain break here but not a
> chain
> > termination
> > TER    3219      GLY A 421
> >
> >
> > TER    3343      GTP C  -1  - Never sure about these but GTP is not part
> of chain
> >
> > TER    4163        G C  37
> > TER    4967        A C  76
> >
> >
> > 2) Some of the atom types are unusual
> >
> > eg  N1+ here instead of N
> >
> > I am not sure whether that is important of not.
> >
> > ATOM     22  NH1 ARG A   4      24.496 181.121 132.218  1.00103.17
>      N1+
> > ANISOU   22  NH1 ARG A   4    15732  10019  13448   1911    785   -419
>      N1+
> >
> >
> >
> >
> > On 10 September 2018 at 10:36, Eleanor Dodson
> > <[email protected] <mailto:[email protected]> > wrote:
> >
> >
> >       Charlie - I will try to check this, but cant read your pse file -
> can you
> > find another format?
> >
> >       Thanks Eleanor
> >
> >
> >       On 8 September 2018 at 12:28, Carter, Charlie <[email protected]
> > <mailto:[email protected]> > wrote:
> >
> >
> >               Hi folks,
> >
> >
> >               I continue to use lsqkab because it offers unique
> flexibility
> > and features appropriate to what I do.
> >
> >
> >               Currently, I’ve a project that requires such superposition
> and
> > for that I created from the original pdb files a set of monomeric pdb
> files that
> > have already been superposed by POSA. The POSA alignment used all the
> > residues, and I want to orient only a subset that is structurally
> invariant, in
> > order to identify possible interdomain motions.
> >
> >
> >               There are ten such files; eight appear to work properly and
> > have aligned. The other two give one or another of two pathologies. The
> first
> > appears simply to get confused and output a rotated coordinate file that
> > appears to be ~90 degrees off, despite the fact that the residue
> numbering is
> > correct (see attached .pse file in which three _Urz coordinate sets are
> > illustrated, which were superimposed on Ecoli_Urz. The Ttherm_H file is
> > correctly rotated; the Stau_LF file is not.).
> >
> >
> >               I decided to try to rotate the two files into an
> intermediate
> > orientation that gave a satisfactory result, i.e. Ttherm_H. The first
> attempt at
> > this involved a second problematic file, Ttherm_tRNA. LSQKSB gave the
> > following error message, which instructs me to contact the developers.
> The
> > problematic pdb file, Ttherm_tRNA.pdb, is also attached.
> >
> >
> >
> >
> >                *** RWBROOK error: point code unit    function
> >                ***                    1 -102    2    MMDB_F_Atom
> >                *** file   : Ttherm_tRNA_rot.pdb
> >                *** reason : internal error #2 -- report to developer
> >                *** Execution stopped.
> >
> >
> >               I should note that I am still using the following version
> of the
> > software:
> >
> >
> >               source  /usr/local/bin/ccp4-7.0/include/ccp4.setup
> >
> >
> >               The commands in my script are:
> >
> >
> >
> >               #source  /usr/local/bin/ccp4-7.0/include/ccp4.setup
> >               lsqkab XYZINM $1 XYZINF $2 XYZOUT $1_rot.pdb << END-
> > lsqkab
> >               FIT RESIDUE MAIN 8 TO 82
> >               MATCH 10 to 84
> >               FIT RESIDUE MAIN 83 TO 111
> >               MATCH 85 to 113
> >               FIT RESIDUE MAIN 122 TO 129
> >               MATCH 124 to 131
> >               OUTPUT XYZ
> >               END
> >               END-lsqkab
> >
> >
> >               Many thanks in advance for any help.
> >
> >
> >
> >
> >
> >
> >
> >
> >
> >
> >
> >
> >
> > ________________________________
> >
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>

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