Hi Almudena, 

did you cut the res. after the merge of your "individual" datasets ? or you cut 
for each and then you merged? 
Because I will probably go for the first, I merge and then I decide where to 
cut. If you cut for each, maybe you "miss" the gain provide by the redundancy 
you have cumulated using all the data. 

If I mis understood what you did, and return a bad answer, sorry. 

And to really answer your question, I will say : I stick to a combination of 
the "standard" stats, CC 1/2 mainly, I/sig and if you expect anomalous, CC Ano 
and SigAno. 
My choice would be conditioned also by the strategy for the phasing. 
Hope to help. 


De: "Almudena Ponce Salvatierra" <[email protected]> 
À: "CCP4BB" <[email protected]> 
Envoyé: Mercredi 4 Novembre 2020 17:30:29 
Objet: [ccp4bb] scale and merge suggestions 

Hello everyone, 
I have collected 6 small datasets from a crystal, each from a different point 
on the crystal to avoid radiation damage, and there is some overlap among them, 
as follows: 

- dts1: 0-90 degrees 
- dts2: 60-150 degrees 
- dts3: 120-210 degrees 
- dts4: 180-270 degrees 
- dts5: 240-330 degrees 
- dts6: 300-390 degrees 

Diffraction is very poor and, after processing, I've cut resolution at around 5 
Angstroms for all of them. The space group is C2. Feeding the 6 of them to 
scale_and_merge in Phenix gives the attached output. Does anybody who has 
merged such low-resolution anomalous data before know whether this is a "good" 
indicator (meaning there's a tiny light at the end of the tunnel) or rather 
not? 

Any suggestions? (besides the obvious "go back to the lab and grow new 
crystals") 

My aim is to combine these phases with a partial molecular replacement solution 
and a native dataset at 3.5 Angstroms. Hopefully, then I would be able to 
finish building the model. 

Thanks a tone in advance! 

Best, 

Almudena 




To unsubscribe from the CCP4BB list, click the following link: 
[ https://www.jiscmail.ac.uk/cgi-bin/WA-JISC.exe?SUBED1=CCP4BB&A=1 | 
https://www.jiscmail.ac.uk/cgi-bin/WA-JISC.exe?SUBED1=CCP4BB&A=1 ] 

########################################################################

To unsubscribe from the CCP4BB list, click the following link:
https://www.jiscmail.ac.uk/cgi-bin/WA-JISC.exe?SUBED1=CCP4BB&A=1

This message was issued to members of www.jiscmail.ac.uk/CCP4BB, a mailing list 
hosted by www.jiscmail.ac.uk, terms & conditions are available at 
https://www.jiscmail.ac.uk/policyandsecurity/

Reply via email to