oh, 1.45 Å is a very short distance for metal coordination. perchlorate has a Cl to O distance of that length https://en.wikipedia.org/wiki/Perchlorate
Mark J van Raaij Dpto de Estructura de Macromoleculas Centro Nacional de Biotecnologia - CSIC calle Darwin 3 E-28049 Madrid, Spain Section Editor Acta Crystallographica F https://journals.iucr.org/f/ > On 26 May 2021, at 15:20, leo john <[email protected]> wrote: > > Hi All: > > Thank You very much for the response and yes it is at symmetry axis. Distance > between the bigger blob and smaller ones is approx 1.45 Ang. > I have tried fitting BO3, BO4, but no luck? > > Thanks > John > > On Wed, May 26, 2021 at 2:14 PM Pearce, N.M. (Nick) <[email protected] > <mailto:[email protected]>> wrote: > Is it on a symmetry axis? If so it could be the superposition of two > molecules (a molecule and a copy of itself). > >> On 26 May 2021, at 15:08, leo john <[email protected] >> <mailto:[email protected]>> wrote: >> >> Hi Group >> Can you please suggest what this unmodeled blob can be (see appended >> picture)? >> I have Malonate, Boric Acid and Peg in my condition, and crystals were >> soaked in GOL. >> >> I have tried fitting PO4 and SO4 so far. >> >> Thank You >> John >> <image.png> >> >> >> >> To unsubscribe from the CCP4BB list, click the following link: >> https://www.jiscmail.ac.uk/cgi-bin/WA-JISC.exe?SUBED1=CCP4BB&A=1 >> <https://www.jiscmail.ac.uk/cgi-bin/WA-JISC.exe?SUBED1=CCP4BB&A=1> > > To unsubscribe from the CCP4BB list, click the following link: > https://www.jiscmail.ac.uk/cgi-bin/WA-JISC.exe?SUBED1=CCP4BB&A=1 > <https://www.jiscmail.ac.uk/cgi-bin/WA-JISC.exe?SUBED1=CCP4BB&A=1> ######################################################################## To unsubscribe from the CCP4BB list, click the following link: https://www.jiscmail.ac.uk/cgi-bin/WA-JISC.exe?SUBED1=CCP4BB&A=1 This message was issued to members of www.jiscmail.ac.uk/CCP4BB, a mailing list hosted by www.jiscmail.ac.uk, terms & conditions are available at https://www.jiscmail.ac.uk/policyandsecurity/
