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The viability of nonaqueous capillary electrophoresis (NACE) was
investigated for determination of gleevec and its main metabolite in human urine
using a fused-silica capillary. Baseline separation of the studied solutes was
obtained using a nonaqueous solution composed of 12 mM ammonium acetate and 87.6
mM acetic acid in methanol-acetonitrile (ACN) (80:20, v:v) providing analysis
time shorter than 3 min.
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