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 1. RE: Non-Aqueous Deacidification Prior to Encapsulation?

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1.From: Valeria Orlandini
 Posted: Saturday November 22, 2025  12:24 PM
 Subject: RE: Non-Aqueous Deacidification Prior to Encapsulation?
 Message: 





Hi Adrienne,
Thanks for posting this interesting inquiry about the use of non-aqueous 
deacidification and encapsulation (re-housing).
I find that it is important to discuss this matter further among conservators 
and conservation scientists.



Note: Deacidification, is a less precise term, which includes the concepts of 
neutralization, alkalization, and sometimes the removal of soluble acidity by 
washing (with full immersion).


Neutralization: Application of an alkaline agent which reacts with acids in 
paper to form a salt.


Alkalization: Application of an alkaline agent which reacts with acids in the 
paper and leaves in paper an alkaline reserve capable of reacting with acids in 
the future. (Because it enables paper to resist changes in pH, an alkaline 
reserve is sometimes called a buffer, and the treatment "buffering".)


BPG Alkalization and Neutralization - MediaWiki 
<https://www.conservation-wiki.com/wiki/BPG_Alkalization_and_Neutralization>


I'd like to know what type of paper-based materials you are planning to treat 
with a non-aqueous deacidification/ alkalization?


Which non-aqueous deacidification method or reagents are you using in your lab?


I agree with Cher's comment: "It's important to remember that deacidification 
spray is preventative, not restorative, and it only provides a superficial 
level of treatment."


It's an intervention where you don't know what the pH of the paper is present 
before and after treatments to allow alkalinization and a deposit of an 
"alkaline reserve." 


Without a full immersion of the paper -- after an aqueous bathing and 
stabilization with an alkaline reserve deposit one cannot measure both 
"quantitative and qualitative" analyses and pHs. 


When a non-aqueous deacidification reagent is applied, there is no way to carry 
out titration as with aqueous deacidification, for example with solutions of 
Calcium bicarbonate and/or Magnesium bicarbonate. 


The efficacy of strengthening and deacidification process(es) in increasing the 
permanence and durability of paper are in question. The permanence increase 
following treatment is found to be strongly dependent upon properties of the 
untreated paper, pH, its strength at the time of treatment, the particular mode 
of strengthening employed, and the process parameters specific to each 
treatment process. 


The Effects of Strengthening and Deacidification on Paper Permanence: Part 
I--some Fundamental Considerations by Donald K. Sebera, Chemist at the Library 
of Congress (1990) The Effects of Strengthening and Deacidification on Paper 
Permanence: Part I -- Some Fundamental Considerations 
<https://cool.culturalheritage.org/coolaic/sg/bpg/annual/v09/bpga09-09.pdf> 


In 2002, I carried out an experiment in Canada to assess various aqueous 
treatments to stabilize ink-corroded materials.


The results and findings of this research addressed and concluded that both 
solutions of deacidification with Ca bicarbonate and Mg bicarbonate used from 
the Library and Archives Canada in Gatineau, Quebec and in conjunction with the 
Canadian Conservation Institute (CCI) in Ottawa, Ontario - didn't leave an 
alkaline reserve deposit after washing. Those samples that were treated with 
alkalinization reached pHs around 7, 7.5 and less with measurements carried out 
in 2002 as well as then recorded with a surface electrode in December 2004 and 
with cold water extractions in June 2006.


Results can be found in the article:  Effect of Aqueous Treatments on 
Nineteenth-Century Iron-Gall-Ink Documents: Calcium Phytate 
Treatment-Optimization of Existing Protocols by Valeria Orlandini, The Book and 
Paper Group Annual 28 (2009) 137-146. bpga28-24.pdf 
<https://cool.culturalheritage.org/coolaic/sg/bpg/annual/v28/bpga28-24.pdf>

Hope to hear your comments and follow up with the discussions.


 <https://cool.culturalheritage.org/coolaic/sg/bpg/annual/v28/bpga28-24.pdf>


Kind regards,


Valeria


P.S. Further inquiries following Sebera's article.











What is the minimum amount of strengthening which is useful and economically 
justifiable? 
Is it adequate to give all papers an equal increase in strength or should the 
weakest papers be strengthened most? 
If strengthening is a one-time event with no change in the rate of paper 
deterioration, how much is the permanence of the paper extended? 
What, if any, are the relationships among paper strengthening, paper 
deacidification and paper permanence?   

Hope the article by John Baty et al entitled DEACIDIFICATION FOR THE 
CONSERVATION AND PRESERVATION OF PAPER-BASED WORKS: A REVIEW will be of 
interest to you.

<[email protected]>

------------------------------
Valeria Orlandini 
Conservator of Works on Paper and Photographic Materials
Chevy Chase MD
(301) 657-2682
------------------------------
-------------------------------------------
Original Message:
Sent: 11-18-2025 11:34
From: Adrienne Bell
Subject: Non-Aqueous Deacidification Prior to Encapsulation?

The Department of Preservation and Conservation Services, University Libraries, 
at the University of North Carolina at Chapel Hill is interested in whether 
institutions are non-aqueously deacidifying materials prior to encapsulation or 
not.  Any research, protocols, or thoughts supporting the decision would be 
appreciated.  Responses can be sent directly to [email protected] 
<[email protected]>; if there is any interest from other institutions, 
responses can be compiled for anonymity and shared.


------------------------------
Adrienne Bell
Senior Conservator
UNC Chapel Hill Libraries
Chapel Hill NC
------------------------------




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